(E,E)-10-tert-butyldiphenylsilyloxy-3,4,8-trimethyl-4,8-decadienal

Base Information

Chemical Name:(E,E)-10-tert-butyldiphenylsilyloxy-3,4,8-trimethyl-4,8-decadienal
CAS No.:250207-23-9
Molecular Formula:C₂₉H₄₀O₂Si
Molecular Weight:448.721
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E,E)-10-tert-butyldiphenylsilyloxy-3,4,8-trimethyl-4,8-decadienal

Chemical Property:

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Technology Process of (E,E)-10-tert-butyldiphenylsilyloxy-3,4,8-trimethyl-4,8-decadienal

There total 7 articles about (E,E)-10-tert-butyldiphenylsilyloxy-3,4,8-trimethyl-4,8-decadienal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-Butyl-((2E,7E)-3,7-dimethyl-6-vinyloxy-nona-2,7-dienyloxy)-diphenyl-silane

: 250207-23-9
(E,E)-10-tert-butyldiphenylsilyloxy-3,4,8-trimethyl-4,8-decadienal

Guidance literature:: In o-xylene; at 140 ℃; for 1h;

Reference yield:

: 106-24-1
Geraniol

: 250207-23-9
(E,E)-10-tert-butyldiphenylsilyloxy-3,4,8-trimethyl-4,8-decadienal

Guidance literature:: Multi-step reaction with 6 steps

1.1: 100 percent / imidazole / dimethylformamide / 1 h / 20 °C

2.1: 89 percent / m-chloroperbenzoic acid / CHCl₃ / 0.5 h / 0 °C

3.1: 86 percent / HIO₄*2H₂O / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C

4.1: tBuLi / pentane; tetrahydrofuran / 2 h / -78 °C

4.2: 67 percent / pentane; tetrahydrofuran / 1 h / -78 °C

5.1: Hg(OAc)2 / 24 h / 20 °C

6.1: o-xylene / 1 h / 140 °C

With 1H-imidazole; mercury(II) diacetate; tert.-butyl lithium; periodic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; chloroform; o-xylene; N,N-dimethyl-formamide; pentane; 1.1: Silylation / 2.1: Epoxidation / 3.1: Oxidation / 4.1: Metallation / 4.2: Alkylation / 5.1: Etherification / 6.1: Rearrangement;

Reference yield:

: 139109-03-8,117638-12-7
tert-butyl ({[(2E)-3,7-dimethylocta-2,6-dien-1-yl]oxy})diphenylsilane

: 250207-23-9
(E,E)-10-tert-butyldiphenylsilyloxy-3,4,8-trimethyl-4,8-decadienal

Guidance literature:: Multi-step reaction with 5 steps

1.1: 89 percent / m-chloroperbenzoic acid / CHCl₃ / 0.5 h / 0 °C

2.1: 86 percent / HIO₄*2H₂O / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C

3.1: tBuLi / pentane; tetrahydrofuran / 2 h / -78 °C

3.2: 67 percent / pentane; tetrahydrofuran / 1 h / -78 °C

4.1: Hg(OAc)2 / 24 h / 20 °C

5.1: o-xylene / 1 h / 140 °C

With mercury(II) diacetate; tert.-butyl lithium; periodic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; chloroform; o-xylene; pentane; 1.1: Epoxidation / 2.1: Oxidation / 3.1: Metallation / 3.2: Alkylation / 4.1: Etherification / 5.1: Rearrangement;