C₂₉H₂₃Cl₂N₅O₅S

Base Information

Chemical Name:C₂₉H₂₃Cl₂N₅O₅S
CAS No.:1432659-52-3
Molecular Formula:C₂₉H₂₃Cl₂N₅O₅S
Molecular Weight:624.504
Hs Code.:

C<sub>29</sub>H<sub>23</sub>Cl<sub>2</sub>N<sub>5</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₂₉H₂₃Cl₂N₅O₅S

Chemical Property:

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Technology Process of C₂₉H₂₃Cl₂N₅O₅S

There total 13 articles about C₂₉H₂₃Cl₂N₅O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₁H₂₇Cl₂N₅O₅S

: 1432659-52-3
C₂₉H₂₃Cl₂N₅O₅S

Guidance literature:: With water; In tetrahydrofuran; methanol; water; at 20 ℃; for 17h;
DOI:10.1002/cmdc.201200474

Reference yield:

: 55432-23-0
cyclopropyl-(2-nitro-phenyl)-amine

: 1432659-52-3
C₂₉H₂₃Cl₂N₅O₅S

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dichloromethane / 72 h / 0 - 20 °C

2.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 900.09 Torr

3.1: borane-THF / tetrahydrofuran / 20 °C

4.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 20 °C

4.2: 20 °C

5.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; carbon monoxide / methanol / 20 h / 100 °C / 52505.3 Torr

6.1: water / methanol; tetrahydrofuran; water / 20 °C

7.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / dichloromethane / 0.25 h / 20 °C

7.2: 4 h / 20 °C

8.1: water / methanol; tetrahydrofuran; water / 17 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; borane-THF; carbon monoxide; palladium 10% on activated carbon; water; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/cmdc.201200474

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1432659-52-3
C₂₉H₂₃Cl₂N₅O₅S

Guidance literature:: Multi-step reaction with 10 steps

1.1: 19 h / 20 - 30 °C

2.1: triethylamine / dichloromethane / 72 h / 0 - 20 °C

3.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 900.09 Torr

4.1: triphenylphosphine / N,N-dimethyl-formamide / 4 h / 135 °C

4.2: 0.5 h / 0 °C

5.1: borane-THF / tetrahydrofuran / 20 °C

6.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 20 °C

6.2: 20 °C

7.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; carbon monoxide / methanol / 20 h / 100 °C / 52505.3 Torr

8.1: water / methanol; tetrahydrofuran; water / 20 °C

9.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / dichloromethane / 0.25 h / 20 °C

9.2: 4 h / 20 °C

10.1: water / methanol; tetrahydrofuran; water / 17 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; borane-THF; carbon monoxide; palladium 10% on activated carbon; water; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201200474