bis{N,N’-{(κ2-P,O)-2-[(tert-butyl-trimethoxyphenyl)phosphine]benzenesulfonate}palladium(II)-methyl}-N,N,N’,N’-tetramethylethylenediamine

Base Information

Chemical Name:bis{N,N’-{(κ2-P,O)-2-[(tert-butyl-trimethoxyphenyl)phosphine]benzenesulfonate}palladium(II)-methyl}-N,N,N’,N’-tetramethylethylenediamine
CAS No.:1488400-98-1
Molecular Formula:C₄₆H₇₀N₂O₁₂P₂Pd₂S₂
Molecular Weight:1181.99
Hs Code.:

bis{N,N’-{(κ2-P,O)-2-[(tert-butyl-trimethoxyphenyl)phosphine]benzenesulfonate}palladium(II)-methyl}-N,N,N’,N’-tetramethylethylenediamine

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Chemical Property of bis{N,N’-{(κ2-P,O)-2-[(tert-butyl-trimethoxyphenyl)phosphine]benzenesulfonate}palladium(II)-methyl}-N,N,N’,N’-tetramethylethylenediamine

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Technology Process of bis{N,N’-{(κ2-P,O)-2-[(tert-butyl-trimethoxyphenyl)phosphine]benzenesulfonate}palladium(II)-methyl}-N,N,N’,N’-tetramethylethylenediamine

There total 6 articles about bis{N,N’-{(κ2-P,O)-2-[(tert-butyl-trimethoxyphenyl)phosphine]benzenesulfonate}palladium(II)-methyl}-N,N,N’,N’-tetramethylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: (N,N,N',N'-tetramethylethylenediamine)dimethylpalladium(II)

: 1449738-99-1
lithium-2-(di-(2,4-dimethoxy-phenyl)phoshine)benzenesulfonic acid

: 1488400-98-1
bis{N,N’-{(κ2-P,O)-2-[(tert-butyl-trimethoxyphenyl)phosphine]benzenesulfonate}palladium(II)-methyl}-N,N,N’,N’-tetramethylethylenediamine

Guidance literature:: In 1,4-dioxane; at 50 ℃; for 2h;
DOI:10.1021/om400297x

Reference yield:

: 621-23-8
1,2,3-trimethoxybenzene

: 1488400-98-1
bis{N,N’-{(κ2-P,O)-2-[(tert-butyl-trimethoxyphenyl)phosphine]benzenesulfonate}palladium(II)-methyl}-N,N,N’,N’-tetramethylethylenediamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N,N,N,-tetramethylethylenediamine / diethyl ether / 12 h / 40 °C / Inert atmosphere; Schlenk technique; Reflux

2.1: N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 12 h / 0 °C / Inert atmosphere; Schlenk technique

2.2: 12 h / 20 °C / Schlenk technique; Inert atmosphere

3.1: tetrahydrofuran / 2 h / 0 °C

3.2: 1.5 h

4.1: water / pH 2

5.1: 1,4-dioxane / 2 h / 50 °C

With N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; 1,4-dioxane; diethyl ether; water;
DOI:10.1021/om400297x

Reference yield:

: 34425-71-3
1-lithium-2,4,6-trimethoxybenzene

: 1488400-98-1
bis{N,N’-{(κ2-P,O)-2-[(tert-butyl-trimethoxyphenyl)phosphine]benzenesulfonate}palladium(II)-methyl}-N,N,N’,N’-tetramethylethylenediamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 12 h / 0 °C / Inert atmosphere; Schlenk technique

1.2: 12 h / 20 °C / Schlenk technique; Inert atmosphere

2.1: tetrahydrofuran / 2 h / 0 °C

2.2: 1.5 h

3.1: water / pH 2

4.1: 1,4-dioxane / 2 h / 50 °C

With N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/om400297x