phenylmethyl <1--3-methylbutyl>carbamate

Base Information

Chemical Name:phenylmethyl <1--3-methylbutyl>carbamate
CAS No.:110582-37-1
Molecular Formula:C₁₄H₂₃N₂O₄P
Molecular Weight:314.321
Hs Code.:

phenylmethyl <1-<amino(methoxy)phosphinyl>-3-methylbutyl>carbamate

Synonyms:

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Chemical Property of phenylmethyl <1--3-methylbutyl>carbamate

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Technology Process of phenylmethyl <1--3-methylbutyl>carbamate

There total 2 articles about phenylmethyl <1--3-methylbutyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: phenylmethyl <1--3-methylbutyl>carbamate

: 110582-37-1,110582-38-2
phenylmethyl <1--3-methylbutyl>carbamate

Guidance literature:: With ammonia; In dichloromethane; at 21 ℃; for 0.166667h;

Reference yield:

: 90763-54-5
methyl <1--3-methylbutyl>phosphonate

: 110582-37-1,110582-38-2
phenylmethyl <1--3-methylbutyl>carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 19 percent / DDPA, triethylamine / CH₂Cl₂ / 18 h / 21 °C

2: 74 percent / ammonia gas / CH₂Cl₂ / 0.17 h / 21 °C

With ammonia; triethylamine; In dichloromethane;

Reference yield:

: 110582-37-1,110582-38-2
phenylmethyl <1--3-methylbutyl>carbamate

: 110582-53-1,110582-54-2
glycyl>-1-amino-3-methylbutyl>(methoxy)phosphonamidate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / H₂ / 10percent Pd/C / methanol / 1 h

2: 50 percent / DPPA, triethylamine / tetrahydrofuran / 0 deg C to 21 deg C

With diphenyl-phosphinic acid; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol;