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dicarbonylbis(triphenylphosphite)sulfurmonoxide iron(0)

Base Information
  • Chemical Name:dicarbonylbis(triphenylphosphite)sulfurmonoxide iron(0)
  • CAS No.:103768-52-1
  • Molecular Formula:C38H30FeO9P2S
  • Molecular Weight:780.511
  • Hs Code.:
dicarbonylbis(triphenylphosphite)sulfurmonoxide iron<sup>(0)</sup>

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Chemical Property of dicarbonylbis(triphenylphosphite)sulfurmonoxide iron(0)
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Technology Process of dicarbonylbis(triphenylphosphite)sulfurmonoxide iron(0)

There total 1 articles about dicarbonylbis(triphenylphosphite)sulfurmonoxide iron(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With triethylamine; thionyl chloride; In petroleum ether; byproducts: [(C2H5)3NH]Cl; under N2; water-free and N2-satd. solvent; excess N(C2H5)3 added to suspn. of dihydrido-complex (30/50°C); cooled to -10°C; soln.of very carefully purified SOCl2 added very slowly by drops; after dissolution (6 h) warmed to room temp.; filtered; washed twice (H2O); dried over P4O10 in high vac.; slowly recrystd. at -30°C (diethyl ether); elem. anal.;
upstream raw materials:

(CO)2(P(OC6H5)3)2FeH2

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