C₃₈H₄₈NO₂PS

Base Information

• Chemical Name: C₃₈H₄₈NO₂PS
• CAS No.: 1616688-64-2
• Molecular Formula: C₃₈H₄₈NO₂PS
• Molecular Weight: 613.844
• Mol file: 1616688-64-2.mol

Synonyms:

Chemical Property of C₃₈H₄₈NO₂PS

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₈H₄₈NO₂PS

There total 6 articles about C₃₈H₄₈NO₂PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-formylphenyl)(diphenyl)phosphine (50777-76-9) → C38H48NO2PS (1616688-64-2) + C38H48NO2PS (1616688-64-2)

Guidance literature:

Multi-step reaction with 2 steps

1: titanium(IV)isopropoxide / tetrahydrofuran / 50 °C / Inert atmosphere

2: dichloromethane; diethyl ether / -48 - 20 °C / Inert atmosphere

With titanium(IV)isopropoxide; In tetrahydrofuran; diethyl ether; dichloromethane;

DOI:10.1002/anie.201401067

Reference yield:

(2-formylphenyl)(diphenyl)phosphine (50777-76-9) → C38H48NO2PS (1616688-64-2) + C38H48NO2PS (1616688-64-2)

Guidance literature:

Multi-step reaction with 2 steps

1: titanium(IV)isopropoxide / tetrahydrofuran / 50 °C / Inert atmosphere

2: dichloromethane; diethyl ether / -48 - 20 °C / Inert atmosphere

With titanium(IV)isopropoxide; In tetrahydrofuran; diethyl ether; dichloromethane;

DOI:10.1002/anie.201401067

Reference yield:

C23H24NOPS + 3,5-di(tert-butyl)-4-methoxyphenylmagnesium bromide → C38H48NO2PS (1616688-64-2) + C38H48NO2PS (1616688-64-2)

Guidance literature:

In diethyl ether; dichloromethane; at -48 - 20 ℃; Overall yield = 90 %; Overall yield = 2.8 g; diastereoselective reaction; Inert atmosphere;

DOI:10.1002/anie.201401067

upstream raw materials:

(2-formylphenyl)(diphenyl)phosphine