1-(3-methyl-3-tert-butylperoxy-1-butynyl)-1-phenyl-1-m-carboranylmethanol

Base Information

Chemical Name:1-(3-methyl-3-tert-butylperoxy-1-butynyl)-1-phenyl-1-m-carboranylmethanol
CAS No.:187797-30-4
Molecular Formula:C₁₈H₃₂B₁₀O₃
Molecular Weight:404.56
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3-methyl-3-tert-butylperoxy-1-butynyl)-1-phenyl-1-m-carboranylmethanol

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Technology Process of 1-(3-methyl-3-tert-butylperoxy-1-butynyl)-1-phenyl-1-m-carboranylmethanol

There total 1 articles about 1-(3-methyl-3-tert-butylperoxy-1-butynyl)-1-phenyl-1-m-carboranylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 29985-59-9
1,7-C₂B₁₀H₁₁-1-COC₆H₅

: 52258-96-5
3-methyl-3-tert-butylperoxy-1-butyne

: 187797-30-4
1-(3-methyl-3-tert-butylperoxy-1-butynyl)-1-phenyl-1-m-carboranylmethanol

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; hexane soln. of BuLi addn. to ether soln. of peroxyalkyne (Ar-atmosphere, -50 to -40°C, 30 min), stirring (15-30 min), ether soln. of carborane addn. (-50 to -40°C, 30 min), stirring (30 min); warming (to room temperature, stirring), staying (18 h), hexane or petroleum ether addn., pouring to ice/water mixture, organic layer sepn., drying (MgSO4), solvent evapn., residue vacuum drying, low-temperature recrystn. from pentane; elem. anal.;