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Technology Process of Rh(NH3)(P(C6H5)3)3(1+)*ClO4(1-)*CH3OH=[Rh(NH3)(P(C6H5)3)3]ClO4*CH3OH

Rh(NH3)(P(C6H5)3)3(1+)*ClO4(1-)*CH3OH=[Rh(NH3)(P(C6H5)3)3]ClO4*CH3OH

Base Information
  • Chemical Name:Rh(NH3)(P(C6H5)3)3(1+)*ClO4(1-)*CH3OH=[Rh(NH3)(P(C6H5)3)3]ClO4*CH3OH
  • CAS No.:157526-60-8
  • Molecular Formula:CH4O*C54H48NP3Rh*ClO4
  • Molecular Weight:1038.3
  • Hs Code.:
Rh(NH<sub>3</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)3<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>*CH<sub>3</sub>OH=[Rh(NH<sub>3</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)3]ClO<sub>4</sub>*CH<sub>3</sub>OH

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Chemical Property of Rh(NH3)(P(C6H5)3)3(1+)*ClO4(1-)*CH3OH=[Rh(NH3)(P(C6H5)3)3]ClO4*CH3OH
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Technology Process of Rh(NH3)(P(C6H5)3)3(1+)*ClO4(1-)*CH3OH=[Rh(NH3)(P(C6H5)3)3]ClO4*CH3OH

There total 1 articles about Rh(NH3)(P(C6H5)3)3(1+)*ClO4(1-)*CH3OH=[Rh(NH3)(P(C6H5)3)3]ClO4*CH3OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

rhodium(III) chloride trihydrate

rhodium(III) chloride trihydrate

silver perchlorate

silver perchlorate

Rh(NH<sub>3</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)3<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>*CH<sub>3</sub>OH=[Rh(NH<sub>3</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)3]ClO<sub>4</sub>*CH<sub>3</sub>OH
157526-60-8

Rh(NH3)(P(C6H5)3)3(1+)*ClO4(1-)*CH3OH=[Rh(NH3)(P(C6H5)3)3]ClO4*CH3OH

Guidance literature:
With P(C6H5)3; NH4F; In methanol; byproducts: AgCl; addn. of solid AgNO3 to methanol soln. of Rh-compd., standing overnight(pptn. of AgCl), filtn., addn. of a methanol soln. of PPh3 (excess) andNH4F, refluxing for 30 min, allowing to cool; crystn. upon storing in a refrigerator (3 d), detn. of purity by (31)P NMR and X-ray crystallography; elem. anal.;
DOI:10.1039/DT9940001857
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