N,N-dimethyl-O-[dichloro(2,2-dimethyl-4-oxobenzo[2H]-1,3-oxazin-3-ylmethyl)germyl]amygdalamide

Base Information

Chemical Name:N,N-dimethyl-O-[dichloro(2,2-dimethyl-4-oxobenzo[2H]-1,3-oxazin-3-ylmethyl)germyl]amygdalamide
CAS No.:917077-22-6
Molecular Formula:C₂₁H₂₄Cl₂GeN₂O₄
Molecular Weight:511.929
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-dimethyl-O-[dichloro(2,2-dimethyl-4-oxobenzo[2H]-1,3-oxazin-3-ylmethyl)germyl]amygdalamide

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Technology Process of N,N-dimethyl-O-[dichloro(2,2-dimethyl-4-oxobenzo[2H]-1,3-oxazin-3-ylmethyl)germyl]amygdalamide

There total 1 articles about N,N-dimethyl-O-[dichloro(2,2-dimethyl-4-oxobenzo[2H]-1,3-oxazin-3-ylmethyl)germyl]amygdalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: N,N-dimethyl-O-[dichloro(chloromethyl)germyl]amygdalamide

: 158567-03-4
2,2-dimethyl-3-(trimethylsilyl)-2H-benzo[e][1,3]oxazin-4-one

: 917077-22-6
N,N-dimethyl-O-[dichloro(2,2-dimethyl-4-oxobenzo[2H]-1,3-oxazin-3-ylmethyl)germyl]amygdalamide

Guidance literature:: In toluene; byproducts: (CH3)3SiCl; mixt. of amide and 2,2-dimethyl-3-trimethylsilylbenzo(2H)-1,3-oxazin-4-onewas refluxed in toluene for 10 h; cooled to room temp.; solvent and Me3SiCl were removed on rotary evaporator; residue crystd. by triturating with ether; elem anal.;
DOI:10.1007/s11172-006-0104-7