dichloro(η-mesitylen)(t-butyldiphenylphosphino)osmium(II)

Base Information

Chemical Name:dichloro(η-mesitylen)(t-butyldiphenylphosphino)osmium(II)
CAS No.:131220-47-8
Molecular Formula:C₂₅H₃₁Cl₂OsP
Molecular Weight:623.601
Hs Code.:

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Chemical Property of dichloro(η-mesitylen)(t-butyldiphenylphosphino)osmium(II)

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Technology Process of dichloro(η-mesitylen)(t-butyldiphenylphosphino)osmium(II)

There total 1 articles about dichloro(η-mesitylen)(t-butyldiphenylphosphino)osmium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: {OsCl2(η-C6H3Me3)}2

: 6002-34-2
tert-butyldiphenylphosphine

: 131220-47-8
dichloro(η-mesitylen)(t-butyldiphenylphosphino)osmium(II)

Guidance literature:: In isopropyl alcohol; refluxed for 4h, cooling; removal of solvent under reduced pressure, recrystn. from CHCl3:ether, NMR, elem. anal.;

Reference yield: 58.0%

: 131220-47-8
dichloro(η-mesitylen)(t-butyldiphenylphosphino)osmium(II)

: 131220-52-5
chloro(hydrido)(η-mesitylene)(t-butyldiphenylphosphino)osmium(II)

Guidance literature:: With sodium carbonate; In isopropyl alcohol; byproducts: (CH3)2CO, NaCl, CO2; heating for 1h; removal of solvent under reduced pressure, crystals from toluene:hexane;

Reference yield: 30.0%

: 16940-66-2
sodium tetrahydroborate

: 131220-47-8
dichloro(η-mesitylen)(t-butyldiphenylphosphino)osmium(II)

: 131220-58-1
dihydrido(η-mesitylene)(t-butyldiphenylphosphine)osmium(II)

Guidance literature:: In isopropyl alcohol; heating overnight; evaporated to dryness, extracted with toluene, chromatography, crystals from ether at -78°C, NMR, IR, elem. anal.;