tetrakis(phenyl vinyl sulfoxide)thorium(IV) bromide

Base Information

Chemical Name:tetrakis(phenyl vinyl sulfoxide)thorium(IV) bromide
CAS No.:152970-18-8
Molecular Formula:C₃₂H₃₂Br₄O₄S₄Th
Molecular Weight:1160.52
Hs Code.:

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Chemical Property of tetrakis(phenyl vinyl sulfoxide)thorium(IV) bromide

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Technology Process of tetrakis(phenyl vinyl sulfoxide)thorium(IV) bromide

There total 1 articles about tetrakis(phenyl vinyl sulfoxide)thorium(IV) bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 20451-53-0
Phenyl vinyl sulfoxide

: 13453-49-1
thorium tetrabromide

: 152970-18-8
tetrakis(phenyl vinyl sulfoxide)thorium(IV) bromide

Guidance literature:: With 2,2-dimethoxypropane; In methanol; dissolution of Th(IV)-salt in abs. MeOH, addn. of 2,2-dimethoxypropane, warming on a water bath (at 80-82°C) with stirring, dropwise addn. of a warm soln. of ligand; pptn. after cooling or after addn. of anhyd. Et2O and stirring for 0.5 h, filtn., washing with MeOH and finally with ether, drying in vacuo over fused CaCl2, elem. anal.;