o-methylbenzyl trifluoroacetate

Base Information

Chemical Name:o-methylbenzyl trifluoroacetate
CAS No.:84658-08-2
Molecular Formula:C₁₀H₉F₃O₂
Molecular Weight:218.175
Hs Code.:

Synonyms:

Suppliers and Price of o-methylbenzyl trifluoroacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of o-methylbenzyl trifluoroacetate

Chemical Property:

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Technology Process of o-methylbenzyl trifluoroacetate

There total 2 articles about o-methylbenzyl trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 89-95-2
2-methyl-benzyl alcohol

: 407-25-0
trifluoroacetic anhydride

: 84658-08-2
o-methylbenzyl trifluoroacetate

Guidance literature:: In diethyl ether; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja304099j

Reference yield: 28.0%

: 89-95-2
2-methyl-benzyl alcohol

: 76-05-1
trifluoroacetic acid

: 84658-08-2
o-methylbenzyl trifluoroacetate

Guidance literature:: a) 20 deg C, 2 h, b) 55 deg C, 2 h;
DOI:10.1002/ijch.199600022

Reference yield:

: 1191-99-7,75454-45-4
2,3-dihydro-2H-furan

: 84658-08-2
o-methylbenzyl trifluoroacetate

: 2-(o-methylbenzyl)-2,5-dihydrofuran.

Guidance literature:: With (+/-)-(5,5',6,6',7,7',8,8'-octahydro-1,1'-binaphthyl)-2,2'-diyl dibenzylphosphoramidite; lithium carbonate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 2-methyltetrahydrofuran; at 40 ℃; for 56h; Inert atmosphere;
DOI:10.1021/ja304099j