methyl>triphenylphosphonium chloride

Base Information

Chemical Name:methyl>triphenylphosphonium chloride
CAS No.:145234-62-4
Molecular Formula:C₄₃H₄₅NO₈P*Cl
Molecular Weight:770.259
Hs Code.:

<Benzyloxycarbonyl-<5-tert-butoxycarbonyl-4-(2-methoxycarbonylethyl)-3-(methoxycarbonylmethyl)pyrrol-2-yl>methyl>triphenylphosphonium chloride

Synonyms:

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Chemical Property of methyl>triphenylphosphonium chloride

Chemical Property:

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Technology Process of methyl>triphenylphosphonium chloride

There total 10 articles about methyl>triphenylphosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66697-04-9
1-tert-butyl, 6-methyl 3-oxo-1,6-hexanedicarboxylate

: 145234-62-4
methyl>triphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 9 steps

1: 1) AcOH, NaNO₂, 2) AcOH, Zn, NaOAc / 1) water, 16 h, 2) 60-65 deg C, 1 h

2: 73 percent / Tl(NO₃)3, conc. HNO₃ / 6 h

3: SO₂Cl₂, K₂CO₃ / CH₂Cl₂ / 1) 0 deg C, 15 min, 2) 20 deg C, 2 h

4: water / acetone / 0.25 h / Heating

5: 96 percent / KI, NaHCO₃, I₂ / CHCl₃; H₂O / 0.42 h / Heating

6: 95 percent / H₂, NaOAc / 10percent Pd/C / methanol / 20 h

7: 25 percent / Cu powder / 0.17 h / 90 °C

8: SO₂Cl₂, K₂CO₃ / CH₂Cl₂ / 0.17 h

9: diethyl ether

With sulfuryl dichloride; water; hydrogen; iodine; nitric acid; sodium acetate; copper; sodium hydrogencarbonate; potassium carbonate; acetic acid; thallium(III) nitrate; potassium iodide; zinc; sodium nitrite; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; chloroform; water; acetone;
DOI:10.1039/P19920002175

Reference yield:

: 113661-72-6
5-Dichloromethyl-3-(2-methoxycarbonyl-ethyl)-4-methoxycarbonylmethyl-1H-pyrrole-2-carboxylic acid tert-butyl ester

: 145234-62-4
methyl>triphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 6 steps

1: water / acetone / 0.25 h / Heating

2: 96 percent / KI, NaHCO₃, I₂ / CHCl₃; H₂O / 0.42 h / Heating

3: 95 percent / H₂, NaOAc / 10percent Pd/C / methanol / 20 h

4: 25 percent / Cu powder / 0.17 h / 90 °C

5: SO₂Cl₂, K₂CO₃ / CH₂Cl₂ / 0.17 h

6: diethyl ether

With sulfuryl dichloride; water; hydrogen; iodine; sodium acetate; copper; sodium hydrogencarbonate; potassium carbonate; potassium iodide; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; chloroform; water; acetone;
DOI:10.1039/P19920002175

Reference yield:

: 118826-20-3
5-tert-Butyl hydrogen 4-(2-methoxycarbonylethyl)-3-(methoxycarbonylmethyl)pyrrole-2,5-dicarboxylate

: 145234-62-4
methyl>triphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / KI, NaHCO₃, I₂ / CHCl₃; H₂O / 0.42 h / Heating

2: 95 percent / H₂, NaOAc / 10percent Pd/C / methanol / 20 h

3: 25 percent / Cu powder / 0.17 h / 90 °C

4: SO₂Cl₂, K₂CO₃ / CH₂Cl₂ / 0.17 h

5: diethyl ether

With sulfuryl dichloride; hydrogen; iodine; sodium acetate; copper; sodium hydrogencarbonate; potassium carbonate; potassium iodide; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; chloroform; water;
DOI:10.1039/P19920002175