{Ru(η5-C5H5)(η5-C5H2Ph3-1,2,3)}

Base Information

Chemical Name:{Ru(η5-C5H5)(η5-C5H2Ph3-1,2,3)}
CAS No.:119071-14-6
Molecular Formula:C₂₈H₂₂Ru
Molecular Weight:459.553
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {Ru(η5-C5H5)(η5-C5H2Ph3-1,2,3)}

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Technology Process of {Ru(η5-C5H5)(η5-C5H2Ph3-1,2,3)}

There total 3 articles about {Ru(η5-C5H5)(η5-C5H2Ph3-1,2,3)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: (cyclooctadienyl)(cyclopentadienyl)ruthenium chloride

: 62747-62-0
1,2,3-triphenyl-3-vinyl-1-cyclopropene

: 119071-14-6
{Ru(η5-C5H5)(η5-C5H2Ph3-1,2,3)}

Guidance literature:: In tetrahydrofuran; soln. of Ru complex treated with the cyclopropene, mixt. stirred (inert atmosphere, room temp., overnight (or 11 d to reach completion), color of soln. changed from orange to golden yellow; solvent removed (vac.), residue extd. with hexanes, recrystd. from Et2O/hexane; elem. anal.;
DOI:10.1021/om00106a023

Reference yield: 75.0%

: (cyclooctadienyl)(cyclopentadienyl)ruthenium chloride

: 119009-88-0
potassium 1,2,3-triphenylcyclopentadienide

: 119071-14-6
{Ru(η5-C5H5)(η5-C5H2Ph3-1,2,3)}

Guidance literature:: In tetrahydrofuran; soln. stirred (inert atmosphere, room temp., 5 h); solvent removed, residue extd. with hexanes or Et2O, recrystd. from these solvents;
DOI:10.1021/om00106a023

Reference yield:

: (cyclooctadienyl)(cyclopentadienyl)ruthenium chloride

: 4982-35-8
1,2,3-triphenylcyclopentadiene

: 119071-14-6
{Ru(η5-C5H5)(η5-C5H2Ph3-1,2,3)}

Guidance literature:: In tetrahydrofuran; soln. stirred (inert atmosphere, room temp.); periodically solvent removed, mixt. taken up in CDCl3 for monitoring the progress of the react. by 1H NMR spect.;
DOI:10.1021/om00106a023