(S)-(3E,5E)-methyl 2-benzoyloxy-2-methyl-3,5-octadienoate

Base Information

Chemical Name:(S)-(3E,5E)-methyl 2-benzoyloxy-2-methyl-3,5-octadienoate
CAS No.:93221-36-4
Molecular Formula:C₁₇H₂₀O₄
Molecular Weight:288.343
Hs Code.:

Synonyms:

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Chemical Property of (S)-(3E,5E)-methyl 2-benzoyloxy-2-methyl-3,5-octadienoate

Chemical Property:

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Technology Process of (S)-(3E,5E)-methyl 2-benzoyloxy-2-methyl-3,5-octadienoate

There total 10 articles about (S)-(3E,5E)-methyl 2-benzoyloxy-2-methyl-3,5-octadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110627-94-6
mevalonic acid

: 93221-36-4
(S)-(3E,5E)-methyl 2-benzoyloxy-2-methyl-3,5-octadienoate

Guidance literature:: Multi-step reaction with 9 steps

1: H₂SO₄ / Ambient temperature

2: pyridine / Ambient temperature

3: BuLi

4: NH₃ / methanol / Ambient temperature

5: pyridinium chlorochromate / CH₂Cl₂ / Ambient temperature

6: molecular sieves 3 Angstroem / benzene / Ambient temperature

7: 2.) H₂O / 1.) THF, -80 deg C, 1 h 2.) 0 geg C, 4 h

8: sodium periodate / tetrahydrofuran; H₂O / Ambient temperature

9: n-BuLi / diethyl ether; hexane

With pyridine; sodium periodate; n-butyllithium; 3 A molecular sieve; sulfuric acid; ammonia; water; pyridinium chlorochromate; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; benzene;

Reference yield:

: 93221-30-8
methyl (S)-2,5-dihydroxy-2-methylpentanoate

: 93221-36-4
(S)-(3E,5E)-methyl 2-benzoyloxy-2-methyl-3,5-octadienoate

Guidance literature:: Multi-step reaction with 8 steps

1: pyridine / Ambient temperature

2: BuLi

3: NH₃ / methanol / Ambient temperature

4: pyridinium chlorochromate / CH₂Cl₂ / Ambient temperature

5: molecular sieves 3 Angstroem / benzene / Ambient temperature

6: 2.) H₂O / 1.) THF, -80 deg C, 1 h 2.) 0 geg C, 4 h

7: sodium periodate / tetrahydrofuran; H₂O / Ambient temperature

8: n-BuLi / diethyl ether; hexane

With pyridine; sodium periodate; n-butyllithium; 3 A molecular sieve; ammonia; water; pyridinium chlorochromate; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; benzene;

Reference yield:

: 93221-31-9
methyl (S)-5-acetoxy-2-hydroxy-2-methylpentanoate

: 93221-36-4
(S)-(3E,5E)-methyl 2-benzoyloxy-2-methyl-3,5-octadienoate

Guidance literature:: Multi-step reaction with 7 steps

1: BuLi

2: NH₃ / methanol / Ambient temperature

3: pyridinium chlorochromate / CH₂Cl₂ / Ambient temperature

4: molecular sieves 3 Angstroem / benzene / Ambient temperature

5: 2.) H₂O / 1.) THF, -80 deg C, 1 h 2.) 0 geg C, 4 h

6: sodium periodate / tetrahydrofuran; H₂O / Ambient temperature

7: n-BuLi / diethyl ether; hexane

With sodium periodate; n-butyllithium; 3 A molecular sieve; ammonia; water; pyridinium chlorochromate; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; benzene;