Os₃(CO)11(P(C₆H₅)2NHC₆H₅)

Base Information

Chemical Name:Os₃(CO)11(P(C₆H₅)2NHC₆H₅)
CAS No.:112312-35-3
Molecular Formula:C₂₉H₁₆NO₁₁Os₃P
Molecular Weight:1156.02
Hs Code.:

Os<sub>3</sub>(CO)11(P(C<sub>6</sub>H<sub>5</sub>)2NHC<sub>6</sub>H<sub>5</sub>)

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Chemical Property of Os₃(CO)11(P(C₆H₅)2NHC₆H₅)

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Technology Process of Os₃(CO)11(P(C₆H₅)2NHC₆H₅)

There total 2 articles about Os₃(CO)11(P(C₆H₅)2NHC₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 133869-39-3,65702-94-5
undecacarbonyl(acetonitrile)triosmium

: 6230-65-5
(diphenylphosphino)phenylamine

: 112312-35-3
Os₃(CO)11(P(C₆H₅)2NHC₆H₅)

Guidance literature:: In dichloromethane; under N2, soln. of Os3(CO)11(NCMe) and PPh2NHPh in CH2Cl2 stirred at room temp. for 15 h; evapd., dissolved in CH2Cl2, TLC (Merck Kieselgel 60 GF 254, C6H12-CH2Cl2 (3:2)), main band extd. with CH2Cl2, recrystd. from pentane;
DOI:10.1016/0022-328X(87)85083-0

Reference yield: 14.0%

: 15696-40-9
dodecacarbonyl triosmium

: 101652-63-5
1,2,2,3,5,6,6,7-octaphenyl-1,3,5,7-tetraaza-2,6-diphosphonia-4,8-diboratacyclooctane

: HOs₃(CO)8(P(C₆H₅)2NHC₆H₅)(P(C₆H₅)2NC₆H₅)

: 112312-35-3
Os₃(CO)11(P(C₆H₅)2NHC₆H₅)

: 112312-36-4
Os₃(CO)10(P(C₆H₅)2NHC₆H₅)2

Guidance literature:: In acetonitrile; under N2, soln. of B-compd. and Os3(CO)12 in MeCN heated to 130°C for 15 h; evapd., dissolved in CH2Cl2, TLC (Merck Kieselgel 60 GF 254, C6H12-CH2Cl2 (3:2)), two yellow bands taken off, extd. with CH2Cl2, again TLC (C6H12-CH2Cl2 (19:1) for upper band; C6H12-CH2Cl2-Et2O (3:1:1) for lower band), extd. with CH2Cl2, recrystd.;
DOI:10.1016/0022-328X(87)85083-0