[TiBr₄((C₆H₅)2AsCH₂CH₂As(C₆H₅)2)]

Base Information

• Chemical Name: [TiBr₄((C₆H₅)2AsCH₂CH₂As(C₆H₅)2)]
• CAS No.: 455253-37-9
• Molecular Formula: C₂₆H₂₄As₂Br₄Ti
• Molecular Weight: 853.816
• Mol file: 455253-37-9.mol

Synonyms:

Chemical Property of [TiBr₄((C₆H₅)2AsCH₂CH₂As(C₆H₅)2)]

Chemical Property:

Purity/Quality:

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Technology Process of [TiBr₄((C₆H₅)2AsCH₂CH₂As(C₆H₅)2)]

There total 1 articles about [TiBr₄((C₆H₅)2AsCH₂CH₂As(C₆H₅)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1,2-bis(diphenylarsino)ethane (4431-24-7) + titanium(IV) bromide (7789-68-6) → [TiBr4((C6H5)2AsCH2CH2As(C6H5)2)] (455253-37-9)

Guidance literature:

In dichloromethane; all manipulations in dry N2 atm.; TiBr4 dissolved in refluxing, dry, degassed CH2Cl2, cooled to room temp., soln. of org. compd. added with stirring, stirred for ca 30 min; solvent vol. reduced, dry, degassed hexane added, filtered, washed with hexane, dried in vac., elem. anal.;

DOI:10.1002/1099-0682(200111)2001:11<2927::AID-EJIC2927>3.0.CO;2-3

upstream raw materials:

1,2-bis(diphenylarsino)ethane

titanium(IV) bromide

Refernces