(2-Fluoro-ethyl)-sulfamic acid (2S,3S)-3-{2-[(Z)-methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-4-oxo-azetidin-2-ylmethyl ester

Base Information

Chemical Name:(2-Fluoro-ethyl)-sulfamic acid (2S,3S)-3-{2-[(Z)-methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-4-oxo-azetidin-2-ylmethyl ester
CAS No.:211515-75-2
Molecular Formula:C₃₁H₃₁FN₆O₆S₂
Molecular Weight:666.754
Hs Code.:

(2-Fluoro-ethyl)-sulfamic acid (2S,3S)-3-{2-[(Z)-methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-4-oxo-azetidin-2-ylmethyl ester

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Chemical Property of (2-Fluoro-ethyl)-sulfamic acid (2S,3S)-3-{2-[(Z)-methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-4-oxo-azetidin-2-ylmethyl ester

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Technology Process of (2-Fluoro-ethyl)-sulfamic acid (2S,3S)-3-{2-[(Z)-methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-4-oxo-azetidin-2-ylmethyl ester

There total 1 articles about (2-Fluoro-ethyl)-sulfamic acid (2S,3S)-3-{2-[(Z)-methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-4-oxo-azetidin-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2-Fluoro-ethyl)-sulfamic acid (2S,3S)-3-amino-4-oxo-azetidin-2-ylmethyl ester; compound with trifluoro-acetic acid

: 64485-90-1
2-(2-aminothiazol-4-yl)-2-(methoxy)iminoacetic acid

: 211515-75-2
(2-Fluoro-ethyl)-sulfamic acid (2S,3S)-3-{2-[(Z)-methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-4-oxo-azetidin-2-ylmethyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; Yield given; 1.) 0 deg C, 2 h, 2.) r.t., 2 h;
DOI:10.1016/S0014-827X(98)00004-4

Reference yield:

: 211515-75-2
(2-Fluoro-ethyl)-sulfamic acid (2S,3S)-3-{2-[(Z)-methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-4-oxo-azetidin-2-ylmethyl ester

: (2S,3S)-2-[(2-Fluoro-ethyl)sulfamoyloxymethyl]-3-{2-[(Z)-methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-4-oxo-azetidine-1-sulfonic acid

Guidance literature:: With sulfur trioxide-N,N-dimethylformamide complex; In N,N-dimethyl-formamide; at 0 ℃; for 1.5h;
DOI:10.1016/S0014-827X(98)00004-4