[Co(benzyl)2(3-[(2-chlorophenyl)ethylimino]-butan-2-one oxime)(3-[(2-pyridyl)ethylimino]-butan-2-one oxime(-1H))]

Base Information

• Chemical Name: [Co(benzyl)2(3-[(2-chlorophenyl)ethylimino]-butan-2-one oxime)(3-[(2-pyridyl)ethylimino]-butan-2-one oxime(-1H))]
• CAS No.: 688360-84-1
• Molecular Formula: C₃₈H₄₃Cl₂CoN₄O₂
• Molecular Weight: 717.684
• Mol file: 688360-84-1.mol

Synonyms:

Chemical Property of [Co(benzyl)2(3-[(2-chlorophenyl)ethylimino]-butan-2-one oxime)(3-[(2-pyridyl)ethylimino]-butan-2-one oxime(-1H))]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Co(benzyl)2(3-[(2-chlorophenyl)ethylimino]-butan-2-one oxime)(3-[(2-pyridyl)ethylimino]-butan-2-one oxime(-1H))]

There total 1 articles about [Co(benzyl)2(3-[(2-chlorophenyl)ethylimino]-butan-2-one oxime)(3-[(2-pyridyl)ethylimino]-butan-2-one oxime(-1H))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

cobalt(II) chloride hexahydrate + 3-[(2-chlorophenyl)ethylimino]-butan-2-one-oxime + benzyl chloride (100-44-7) → [Co(benzyl)2(3-[(2-chlorophenyl)ethylimino]-butan-2-one oxime)(3-[(2-pyridyl)ethylimino]-butan-2-one oxime(-1H))] (688360-84-1)

Guidance literature:

With NaBH₄; PdCl₂; HCl; In ethanol; water; mixt. of CoCl2*6H2O and oxime ligand in EtOH treated under N2 atm. and vigorous stirring with NaBH4 and benzylchloride; a drop PdCl2 added; vessel placed in ice bath; ppt. collected by filtration; washed (H2O); dried (air); crystn. was performed by addition of isopropyl ether to satd. THF soln.; soln. allowed to stand overnight; elem. anal.;

DOI:10.1016/S0020-1693(03)00429-8

upstream raw materials:

benzyl chloride