[(1-phenyl-3,5-dimethylpyrazole-H)2Ir(3-phenyl-5-(2-pyridyl)pyrazole)]

Base Information

Chemical Name:[(1-phenyl-3,5-dimethylpyrazole-H)2Ir(3-phenyl-5-(2-pyridyl)pyrazole)]
CAS No.:959906-78-6
Molecular Formula:C₃₆H₃₂IrN₇
Molecular Weight:754.917
Hs Code.:

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Chemical Property of [(1-phenyl-3,5-dimethylpyrazole-H)2Ir(3-phenyl-5-(2-pyridyl)pyrazole)]

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Technology Process of [(1-phenyl-3,5-dimethylpyrazole-H)2Ir(3-phenyl-5-(2-pyridyl)pyrazole)]

There total 2 articles about [(1-phenyl-3,5-dimethylpyrazole-H)2Ir(3-phenyl-5-(2-pyridyl)pyrazole)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: [(1-phenyl-3,5-dimethylpyrazole-H)2IrCl]2

: 15395-62-7
2-(3-phenyl-1H-pyrazol-5-yl) pyridine

: 959906-78-6
[(1-phenyl-3,5-dimethylpyrazole-H)2Ir(3-phenyl-5-(2-pyridyl)pyrazole)]

Guidance literature:: With Na₂CO₃; In further solvent(s); under N2, Ir-compd. and 2 equiv. of N-compd. were refluxed with excess of Na2CO3 for 6 h in 2-methoxyethanol; cooling to room temp., excess of H2O was added, ppt. was filtered off and subjected to silica gel column chromy. (EtOAc-MeOH=9:1), repeated recrystn. from THF-pentane at room temp., elem. anal.;
DOI:10.1016/j.poly.2007.06.029

Reference yield:

: 1131-16-4
3,5-dimethyl-1-phenyl-1H-pyrazole

: 959906-78-6
[(1-phenyl-3,5-dimethylpyrazole-H)2Ir(3-phenyl-5-(2-pyridyl)pyrazole)]

Guidance literature:: Multi-step reaction with 2 steps

1: further solvent(s)

2: Na₂CO₃ / further solvent(s)

With Na₂CO₃; In further solvent(s);
DOI:10.1016/j.poly.2007.06.029