Technology Process of C17H23NO4
There total 4 articles about C17H23NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: C38H25BO3; C44H30B2O5; (2S)-(-)-3,3'-diphenyl-(2,2'-binaphthalene)-1,1'-diol / toluene / 25 °C
2.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere
2.2: 2 h / -78 - 20 °C / Inert atmosphere
3.1: trifluorormethanesulfonic acid; methoxybenzene / 0.75 h / 0 - 20 °C
4.1: sodium hydrogencarbonate / methanol / 5 h / Sonication
With
trifluorormethanesulfonic acid; C38H25BO3; C44H30B2O5; sodium hydrogencarbonate; methoxybenzene; lithium diisopropyl amide; (2S)-(-)-3,3'-diphenyl-(2,2'-binaphthalene)-1,1'-diol;
In
tetrahydrofuran; methanol; hexane; toluene;
DOI:10.1021/ja203754p
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trifluorormethanesulfonic acid; methoxybenzene / 0.75 h / 0 - 20 °C
2: sodium hydrogencarbonate / methanol / 5 h / Sonication
With
trifluorormethanesulfonic acid; sodium hydrogencarbonate; methoxybenzene;
In
methanol;
DOI:10.1021/ja203754p
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere
1.2: 2 h / -78 - 20 °C / Inert atmosphere
2.1: trifluorormethanesulfonic acid; methoxybenzene / 0.75 h / 0 - 20 °C
3.1: sodium hydrogencarbonate / methanol / 5 h / Sonication
With
trifluorormethanesulfonic acid; sodium hydrogencarbonate; methoxybenzene; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; hexane;
DOI:10.1021/ja203754p