2-(α-benzoylaminobutanoic acid)-2-methyl-1,3-dioxolane ethyl ester

Base Information

Chemical Name:2-(α-benzoylaminobutanoic acid)-2-methyl-1,3-dioxolane ethyl ester
CAS No.:79195-06-5
Molecular Formula:C₁₇H₂₃NO₅
Molecular Weight:321.373
Hs Code.:

Synonyms:

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Chemical Property of 2-(α-benzoylaminobutanoic acid)-2-methyl-1,3-dioxolane ethyl ester

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Technology Process of 2-(α-benzoylaminobutanoic acid)-2-methyl-1,3-dioxolane ethyl ester

There total 1 articles about 2-(α-benzoylaminobutanoic acid)-2-methyl-1,3-dioxolane ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79195-02-1
2-methyl-2-(α-nitrobutanoic acid)-1,3-dioxolane ethyl ester

: 79195-06-5
2-(α-benzoylaminobutanoic acid)-2-methyl-1,3-dioxolane ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / H₂ / Pd/c / aq. ethanol / 10 h / 50 °C / 77572.2 Torr

2: 50.7 percent / pyridine / benzene / 0.5 h / Heating

With pyridine; hydrogen; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1002/jps.2600700508

Reference yield:

: 79195-06-5
2-(α-benzoylaminobutanoic acid)-2-methyl-1,3-dioxolane ethyl ester

: 79195-08-7
N-(3-hydroxy-1-oxo-2-cyclohexen-4-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / Ambient temperature

2: 1.) NaH, 2.) aq. HCl / 1) benzene, 50 - 60 deg C (1 h), reflux (5 h)

With hydrogenchloride; sodium hydride;
DOI:10.1002/jps.2600700508

Reference yield:

: 79195-06-5
2-(α-benzoylaminobutanoic acid)-2-methyl-1,3-dioxolane ethyl ester

: N-(3-ethoxy-1-oxo-2-cyclohexen-6-yl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: aq. HCl / Ambient temperature

2: 1.) NaH, 2.) aq. HCl / 1) benzene, 50 - 60 deg C (1 h), reflux (5 h)

3: 39.8 percent / N,N,N'N'-tetramethyl-1,8-naphthalenediamine / 1) CH₂Cl₂, 4 h; 2) CH₂Cl₂, methanol, 10 h

With hydrogenchloride; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; sodium hydride;
DOI:10.1002/jps.2600700508