C₅H₅Ru(CO)(P(OC₆H₅)3)NO₃

Base Information

• Chemical Name: C₅H₅Ru(CO)(P(OC₆H₅)3)NO₃
• CAS No.: 348625-01-4
• Molecular Formula: C₂₄H₂₀NO₇PRu
• Molecular Weight: 566.469
• Mol file: 348625-01-4.mol

Synonyms:

Chemical Property of C₅H₅Ru(CO)(P(OC₆H₅)3)NO₃

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₅H₅Ru(CO)(P(OC₆H₅)3)NO₃

There total 1 articles about C₅H₅Ru(CO)(P(OC₆H₅)3)NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

C5H5Ru(CO)(P(OC6H5)3)Cl (32611-29-3) + silver nitrate → C5H5Ru(CO)(P(OC6H5)3)NO3 (348625-01-4)

Guidance literature:

In toluene; the mixt. in toluene was heated under N2 at reflux for 30 h; concd., diethyl ether was added dropwise, then heptane, ppt. was filtered, washed with heptane, dried overnight in vac.;

DOI:10.1021/om000670d

Reference yield: 99.0%

C5H5Ru(CO)(P(OC6H5)3)NO3 (348625-01-4) + bis(triphenylphosphine)iminium chloride (21050-13-5) → bis(triphenylphosphine)iminium nitrate (38011-35-7) + C5H5Ru(CO)(P(OC6H5)3)Cl (32611-29-3)

Guidance literature:

In dichloromethane; 25°C, CH2Cl2; not sepd., detected by UV spectra; Kinetics;

DOI:10.1021/om000670d

upstream raw materials:

C₅H₅Ru(CO)(P(OC₆H₅)3)Cl

Downstream raw materials:

bis(triphenylphosphine)iminium nitrate

C₅H₅Ru(CO)(P(OC₆H₅)3)Cl