3-[(S)-3-Benzyloxycarbonylamino-2-(3-{(S)-3-benzyloxycarbonylamino-2-[3-((S)-3-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-propionylamino)-benzoylamino]-propionylamino}-benzoylamino)-propionylamino]-benzoic acid

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Chemical Name:3-[(S)-3-Benzyloxycarbonylamino-2-(3-{(S)-3-benzyloxycarbonylamino-2-[3-((S)-3-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-propionylamino)-benzoylamino]-propionylamino}-benzoylamino)-propionylamino]-benzoic acid
CAS No.:244787-60-8
Molecular Formula:C₅₉H₆₁N₉O₁₅
Molecular Weight:1136.18
Hs Code.:

3-[(S)-3-Benzyloxycarbonylamino-2-(3-{(S)-3-benzyloxycarbonylamino-2-[3-((S)-3-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-propionylamino)-benzoylamino]-propionylamino}-benzoylamino)-propionylamino]-benzoic acid

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Chemical Property of 3-[(S)-3-Benzyloxycarbonylamino-2-(3-{(S)-3-benzyloxycarbonylamino-2-[3-((S)-3-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-propionylamino)-benzoylamino]-propionylamino}-benzoylamino)-propionylamino]-benzoic acid

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Technology Process of 3-[(S)-3-Benzyloxycarbonylamino-2-(3-{(S)-3-benzyloxycarbonylamino-2-[3-((S)-3-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-propionylamino)-benzoylamino]-propionylamino}-benzoylamino)-propionylamino]-benzoic acid

There total 1 articles about 3-[(S)-3-Benzyloxycarbonylamino-2-(3-{(S)-3-benzyloxycarbonylamino-2-[3-((S)-3-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-propionylamino)-benzoylamino]-propionylamino}-benzoylamino)-propionylamino]-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 226982-42-9
3-[(S)-3-Benzyloxycarbonylamino-2-(3-{(S)-3-benzyloxycarbonylamino-2-[3-((S)-3-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-propionylamino)-benzoylamino]-propionylamino}-benzoylamino)-propionylamino]-benzoic acid 2-oxo-2-phenyl-ethyl ester

: 244787-60-8
3-[(S)-3-Benzyloxycarbonylamino-2-(3-{(S)-3-benzyloxycarbonylamino-2-[3-((S)-3-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-propionylamino)-benzoylamino]-propionylamino}-benzoylamino)-propionylamino]-benzoic acid

Guidance literature:: With acetic acid; zinc; for 4h; Ambient temperature;
DOI:10.1016/S0040-4039(99)00544-4

Reference yield: 99.0%

: 76-05-1
trifluoroacetic acid

: 244787-60-8
3-[(S)-3-Benzyloxycarbonylamino-2-(3-{(S)-3-benzyloxycarbonylamino-2-[3-((S)-3-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-propionylamino)-benzoylamino]-propionylamino}-benzoylamino)-propionylamino]-benzoic acid

: 3-[(S)-2-(3-{(S)-2-[3-((S)-2-Amino-3-benzyloxycarbonylamino-propionylamino)-benzoylamino]-3-benzyloxycarbonylamino-propionylamino}-benzoylamino)-3-benzyloxycarbonylamino-propionylamino]-benzoic acid; compound with trifluoro-acetic acid

Guidance literature:: In chloroform; for 1h; Ambient temperature;
DOI:10.1016/S0040-4039(99)00544-4

Reference yield:

: 244787-60-8
3-[(S)-3-Benzyloxycarbonylamino-2-(3-{(S)-3-benzyloxycarbonylamino-2-[3-((S)-3-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-propionylamino)-benzoylamino]-propionylamino}-benzoylamino)-propionylamino]-benzoic acid

: 226982-45-2
C₅₄H₅₁N₉O₁₂

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / CHCl₃ / 1 h / Ambient temperature

2: 60 percent / DPPA, DIEA / dimethylformamide / 16 h / Ambient temperature

With diphenyl-phosphinic acid; N-ethyl-N,N-diisopropylamine; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(99)00544-4