Technology Process of C57H78F3N3O29
There total 11 articles about C57H78F3N3O29 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: titanium(IV) bromide / dichloromethane / 3 h / 20 °C
2: silver trifluoromethanesulfonate; tetramethylurea / dichloromethane / 20 h / 20 °C / Molecular sieve
3: water; triphenylphosphine / tetrahydrofuran / 16 h
4: 1 h
With
water; silver trifluoromethanesulfonate; titanium(IV) bromide; triphenylphosphine; tetramethylurea;
In
tetrahydrofuran; dichloromethane;
DOI:10.1055/s-0032-1317961
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 1,2-dichloro-ethane
2: sodium azide / dimethyl sulfoxide / 80 °C
3: sodium methylate; methanol
4: toluene-4-sulfonic acid / acetonitrile
5: pyridine
6: sodium cyanoborohydride; methanesulfonic acid / tetrahydrofuran
7: silver trifluoromethanesulfonate; tetramethylurea / dichloromethane / 20 h / 20 °C / Molecular sieve
8: water; triphenylphosphine / tetrahydrofuran / 16 h
9: 1 h
With
pyridine; methanol; sodium azide; methanesulfonic acid; water; sodium methylate; silver trifluoromethanesulfonate; sodium cyanoborohydride; toluene-4-sulfonic acid; triphenylphosphine; tetramethylurea;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1055/s-0032-1317961
- Guidance literature:
-
Multi-step reaction with 8 steps
1: sodium azide / dimethyl sulfoxide / 80 °C
2: sodium methylate; methanol
3: toluene-4-sulfonic acid / acetonitrile
4: pyridine
5: sodium cyanoborohydride; methanesulfonic acid / tetrahydrofuran
6: silver trifluoromethanesulfonate; tetramethylurea / dichloromethane / 20 h / 20 °C / Molecular sieve
7: water; triphenylphosphine / tetrahydrofuran / 16 h
8: 1 h
With
pyridine; methanol; sodium azide; methanesulfonic acid; water; sodium methylate; silver trifluoromethanesulfonate; sodium cyanoborohydride; toluene-4-sulfonic acid; triphenylphosphine; tetramethylurea;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1055/s-0032-1317961