[(2-Me-9-((CH₂)4OC(O)CH₂OC(O)C(C₆₀)COOCH₂C₆H₃(OC₁₂H₂₅)2)-1,10-phenanthroline)(bis[2-diphenylphosphino)phenyl]ether)copper(I)]BF₄

Base Information

• Chemical Name: [(2-Me-9-((CH₂)4OC(O)CH₂OC(O)C(C₆₀)COOCH₂C₆H₃(OC₁₂H₂₅)2)-1,10-phenanthroline)(bis[2-diphenylphosphino)phenyl]ether)copper(I)]BF₄
• CAS No.: 1042688-47-0
• Molecular Formula: BF₄*C₁₄₉H₁₀₂CuN₂O₉P₂
• Molecular Weight: 2276.76
• Mol file: 1042688-47-0.mol

Synonyms:

Chemical Property of [(2-Me-9-((CH₂)4OC(O)CH₂OC(O)C(C₆₀)COOCH₂C₆H₃(OC₁₂H₂₅)2)-1,10-phenanthroline)(bis[2-diphenylphosphino)phenyl]ether)copper(I)]BF₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(2-Me-9-((CH₂)4OC(O)CH₂OC(O)C(C₆₀)COOCH₂C₆H₃(OC₁₂H₂₅)2)-1,10-phenanthroline)(bis[2-diphenylphosphino)phenyl]ether)copper(I)]BF₄

There total 1 articles about [(2-Me-9-((CH₂)4OC(O)CH₂OC(O)C(C₆₀)COOCH₂C₆H₃(OC₁₂H₂₅)2)-1,10-phenanthroline)(bis[2-diphenylphosphino)phenyl]ether)copper(I)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

tetrakis(acetonitrile)copper(I)tetrafluoroborate + N2C12H6(CH3)(CH2)4OC(O)CH2OC(O)C(C60)C(O)OCH2C6H3(OC12H25)2 (1042742-42-6) + bis[2-(diphenylphosphino)phenyl] ether (166330-10-5) → [(2-Me-9-((CH2)4OC(O)CH2OC(O)C(C60)COOCH2C6H3(OC12H25)2)-1,10-phenanthroline)(bis[2-diphenylphosphino)phenyl]ether)copper(I)]BF4 (1042688-47-0)

Guidance literature:

In dichloromethane; Cu complex added to stirred soln. of diphosphine in CH2Cl2; stirred at 25°C for 1 h; soln. of susbstituted phenanthroline ligand in CH2Cl2 added; stirred for 2 h; evapd.; purified by gel permeation chromy. (silica gel, CH2Cl2); elem. anal.;

DOI:10.1021/ic800315e

upstream raw materials:

N₂C₁₂H₆(CH₃)(CH₂)4OC(O)CH₂OC(O)C(C₆₀)C(O)OCH₂C₆H₃(OC₁₂H₂₅)2

bis[2-(diphenylphosphino)phenyl] ether