6(R),13(RS)-dibenzoyloxy-tetradeca-2(E),4(E),8(Z)-trienal

Base Information

Chemical Name:6(R),13(RS)-dibenzoyloxy-tetradeca-2(E),4(E),8(Z)-trienal
CAS No.:117567-67-6
Molecular Formula:C₂₈H₃₀O₅
Molecular Weight:446.543
Hs Code.:

Synonyms:

Suppliers and Price of 6(R),13(RS)-dibenzoyloxy-tetradeca-2(E),4(E),8(Z)-trienal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6(R),13(RS)-dibenzoyloxy-tetradeca-2(E),4(E),8(Z)-trienal

Chemical Property:

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Technology Process of 6(R),13(RS)-dibenzoyloxy-tetradeca-2(E),4(E),8(Z)-trienal

There total 11 articles about 6(R),13(RS)-dibenzoyloxy-tetradeca-2(E),4(E),8(Z)-trienal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₇H₁₀LiO^(1-)*Li⁽¹⁺⁾

: 117567-67-6,117567-77-8,134268-91-0,134268-96-5
6(R),13(RS)-dibenzoyloxy-tetradeca-2(E),4(E),8(Z)-trienal

Guidance literature:: Multi-step reaction with 5 steps

1: 1) THF, HMPT, a) 65 deg C, 6 h, b) room temp., 15 h, 2) 0 deg C, 35 min

2: 74 percent / H₂ / Pd/CaCO₃/Pb / benzene / 5 h / Ambient temperature

3: 99 percent / trifluoroacetic acid / H₂O / 1 h / 0 °C

4: 86 percent / Pb(OAc)4 / CH₂Cl₂ / 1.25 h / -10 °C

5: K₂CO₃ / tetrahydrofuran; diethyl ether; H₂O / 23 h / Ambient temperature

With lead(IV) acetate; hydrogen; potassium carbonate; trifluoroacetic acid; Lindlar's catalyst; In tetrahydrofuran; diethyl ether; dichloromethane; water; benzene;

Reference yield:

: 134268-86-3
2(RS),9(R),12(R),19(RS)-tetrabenzoyloxy-10(R),11(R)-O-isopropylidene-icosa-6,14-diyne-10,11-diol

: 117567-67-6,117567-77-8,134268-91-0,134268-96-5
6(R),13(RS)-dibenzoyloxy-tetradeca-2(E),4(E),8(Z)-trienal

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / H₂ / Pd/CaCO₃/Pb / benzene / 5 h / Ambient temperature

2: 99 percent / trifluoroacetic acid / H₂O / 1 h / 0 °C

3: 86 percent / Pb(OAc)4 / CH₂Cl₂ / 1.25 h / -10 °C

4: K₂CO₃ / tetrahydrofuran; diethyl ether; H₂O / 23 h / Ambient temperature

With lead(IV) acetate; hydrogen; potassium carbonate; trifluoroacetic acid; Lindlar's catalyst; In tetrahydrofuran; diethyl ether; dichloromethane; water; benzene;

Reference yield:

: C₇H₁₀LiO^(1-)*Li⁽¹⁺⁾

: 117567-67-6,117567-77-8,134268-91-0,134268-96-5
6(R),13(RS)-dibenzoyloxy-tetradeca-2(E),4(Z),8(Z)-trienal

Guidance literature:: Multi-step reaction with 5 steps

1: 1) THF, HMPT, a) 65 deg C, 6 h, b) room temp., 15 h, 2) 0 deg C, 35 min

2: 74 percent / H₂ / Pd/CaCO₃/Pb / benzene / 5 h / Ambient temperature

3: 99 percent / trifluoroacetic acid / H₂O / 1 h / 0 °C

4: 86 percent / Pb(OAc)4 / CH₂Cl₂ / 1.25 h / -10 °C

5: K₂CO₃ / tetrahydrofuran; diethyl ether; H₂O / 23 h / Ambient temperature

With lead(IV) acetate; hydrogen; potassium carbonate; trifluoroacetic acid; Lindlar's catalyst; In tetrahydrofuran; diethyl ether; dichloromethane; water; benzene;