humulene 2,3-epoxide

Base Information

• Chemical Name: humulene 2,3-epoxide
• CAS No.: 80797-01-9
• Molecular Formula: C₁₅H₂₄O
• Molecular Weight: 220.355

Synonyms:

Chemical Property of humulene 2,3-epoxide

Chemical Property:

Purity/Quality:

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Technology Process of humulene 2,3-epoxide

There total 5 articles about humulene 2,3-epoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

α-caryophyllene (6753-98-6) → (3E,7E)-1,5,5,8-tetramethyl-12-oxabicyclo[9.1.0]dodeca-3,7-diene (882187-46-4,831227-95-3) + humulene 2,3-epoxide (19888-33-6,74282-07-8,80409-05-8,80797-01-9) + 9S*,10S*-humulene 9,10-epoxide

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; at -10 - 20 ℃; for 15h; regioselective reaction;

DOI:10.1002/anie.201502302

Reference yield: 15.0%

α-caryophyllene (6753-98-6) → humulene 2,3-epoxide (19888-33-6,74282-07-8,80409-05-8,80797-01-9)

Guidance literature:

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In tetrachloromethane;

DOI:10.1016/S0040-4039(00)71413-4

Reference yield:

(9E)-humulene-2,3;6,7-diepoxide (531492-87-2) → (3E,7E)-1,5,5,8-tetramethyl-12-oxabicyclo[9.1.0]dodeca-3,7-diene (882187-46-4,831227-95-3) + α-caryophyllene (6753-98-6) + humulene 2,3-epoxide (19888-33-6,74282-07-8,80409-05-8,80797-01-9)

Guidance literature:

With lithium aluminium tetrahydride; titanium(III) chloride; In tetrahydrofuran; at 10 - 20 ℃; for 0.583333h;

DOI:10.3987/COM-01-S1

upstream raw materials:

α-caryophyllene

(9E)-humulene-2,3;6,7-diepoxide

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