C₂₉H₂₂ClN₂O₄S^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₂₉H₂₂ClN₂O₄S^(1-)*Na⁽¹⁺⁾
CAS No.:1423691-17-1
Molecular Formula:C₂₉H₂₂ClN₂O₄S*Na
Molecular Weight:553.013
Hs Code.:

C<sub>29</sub>H<sub>22</sub>ClN<sub>2</sub>O<sub>4</sub>S<sup>(1-)</sup>*Na<sup>(1+)</sup>

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Chemical Property of C₂₉H₂₂ClN₂O₄S^(1-)*Na⁽¹⁺⁾

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Technology Process of C₂₉H₂₂ClN₂O₄S^(1-)*Na⁽¹⁺⁾

There total 5 articles about C₂₉H₂₂ClN₂O₄S^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2142-68-9
1-(2-chlorophenyl)ethanone

: 1423691-17-1
C₂₉H₂₂ClN₂O₄S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 5 steps

1.1: (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; dimethylsulfide borane complex / tetrahydrofuran / 0.5 h / 20 °C

2.1: diphenyl phosphoryl azide; triethylamine / toluene / 1 h / Reflux; Inert atmosphere

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere

4.1: sodium t-butanolate / tetrahydrofuran; acetonitrile / 20 °C

4.2: 0 °C / pH 4.0

5.1: sodium hydroxide / acetonitrile / 0.5 h / 0 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; dimethylsulfide borane complex; diphenyl phosphoryl azide; sodium carbonate; triethylamine; sodium hydroxide; sodium t-butanolate; (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; In tetrahydrofuran; 1,2-dimethoxyethane; water; toluene; acetonitrile;

Reference yield:

: 13524-04-4,131864-71-6,132437-66-2,120466-66-2
(R)-1-(o-chlorophenyl)ethanol

: 1423691-17-1
C₂₉H₂₂ClN₂O₄S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 4 steps

1.1: diphenyl phosphoryl azide; triethylamine / toluene / 1 h / Reflux; Inert atmosphere

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere

3.1: sodium t-butanolate / tetrahydrofuran; acetonitrile / 20 °C

3.2: 0 °C / pH 4.0

4.1: sodium hydroxide / acetonitrile / 0.5 h / 0 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; diphenyl phosphoryl azide; sodium carbonate; triethylamine; sodium hydroxide; sodium t-butanolate; In tetrahydrofuran; 1,2-dimethoxyethane; water; toluene; acetonitrile;

Reference yield:

: 1423691-14-8
C₃₀H₂₅ClN₂O₄S

: 1423691-17-1
C₂₉H₂₂ClN₂O₄S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium t-butanolate / tetrahydrofuran; acetonitrile / 20 °C

1.2: 0 °C / pH 4.0

2.1: sodium hydroxide / acetonitrile / 0.5 h / 0 °C

With sodium hydroxide; sodium t-butanolate; In tetrahydrofuran; acetonitrile;