(carbonyl)7(triphenylphosphine)3(ruthenium)2platinum

Base Information

Chemical Name:(carbonyl)7(triphenylphosphine)3(ruthenium)2platinum
CAS No.:82441-41-6
Molecular Formula:C₆₁H₄₅O₇P₃PtRu₂
Molecular Weight:1380.17
Hs Code.:

Synonyms:

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Chemical Property of (carbonyl)7(triphenylphosphine)3(ruthenium)2platinum

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Technology Process of (carbonyl)7(triphenylphosphine)3(ruthenium)2platinum

There total 3 articles about (carbonyl)7(triphenylphosphine)3(ruthenium)2platinum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 12120-15-9
ethylenebis(triphenylphosphine)platinum⁽⁰⁾

: 69403-55-0,89397-37-5
Ru₃(carbonyl)11(t-butyl isocyanide)

: 205441-17-4
Ru₃(CO)11(PPh₃)

: 82441-41-6
(carbonyl)7(triphenylphosphine)3(ruthenium)2platinum

: 34852-58-9
[Pt₂Ru(CO)₂(μ-CO)₃(PPh₃)₃]

: 82441-43-8
(carbonyl)6(t-butyl isocyanide)(triphenylphosphine)(ruthenium)(platinum)2

: (carbonyl)9(t-butyl isocyanide)(triphenylphosphine)(ruthenium)2platinum

Guidance literature:: With CO; In toluene; mixing toluene solns. of Ru-complex and Pt-complex at -20°C under N2, bubbling CO through this soln. for 30 min at -20°C, colour of soln. changes to yellow-orange; sepn. of products by preparative TLC (ether/cyclohexane) gives an orange band and three further products, further sepn. of orange band gives two compds. (total yield: 19%), elem. anal.;

Reference yield: 33.0%

: 12120-15-9
ethylenebis(triphenylphosphine)platinum⁽⁰⁾

: 69403-55-0,89397-37-5
Ru₃(carbonyl)11(t-butyl isocyanide)

: 205441-17-4
Ru₃(CO)11(PPh₃)

: 82441-41-6
(carbonyl)7(triphenylphosphine)3(ruthenium)2platinum

: 34852-58-9
[Pt₂Ru(CO)₂(μ-CO)₃(PPh₃)₃]

: (carbonyl)9(t-butyl isocyanide)(triphenylphosphine)(ruthenium)2platinum

: 83343-68-4
(carbonyl)10(t-butyl isocyanide)(triphenylphosphine)(ruthenium)3

Guidance literature:: In methyl cyclohexane; mixing solns. of Ru-complex and Pt-complex in methylcyclohexane at roomtemp. under N2, colour changes to deep red within 5 s, stirring at roomtemp. for 120 min; removal of solvent under vacuum, preparative TLC (acetone petroleum ether), several bands, further purification (TLC, recrystn.) affords 6 products, elem. anal.;

Reference yield: 25.0%

: 12120-15-9
ethylenebis(triphenylphosphine)platinum⁽⁰⁾

: 69403-55-0,89397-37-5
Ru₃(carbonyl)11(t-butyl isocyanide)

: 205441-17-4
Ru₃(CO)11(PPh₃)

: 82441-41-6
(carbonyl)7(triphenylphosphine)3(ruthenium)2platinum

: 82441-43-8
(carbonyl)6(t-butyl isocyanide)(triphenylphosphine)(ruthenium)(platinum)2

: (carbonyl)9(t-butyl isocyanide)(triphenylphosphine)(ruthenium)2platinum

: 83343-68-4
(carbonyl)10(t-butyl isocyanide)(triphenylphosphine)(ruthenium)3

Guidance literature:: In benzene; mixing solns. of Ru-complex and Pt-complex in benzene at room temp. under N2, colour changes to deep red within 5 s, stirring at room temp. for30 min; removal of solvent under vacuum, preparative TLC (acetone petroleum ether), thirteen bands, further purification (TLC, recrystn.) affords 6 products, elem. anal.;