Technology Process of C26H27N3OS
There total 8 articles about C26H27N3OS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
ethanol; toluene;
at 95 - 100 ℃;
for 24h;
DOI:10.1016/j.bmcl.2013.05.025
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2,6-dimethylpyridine / ethanol / 90 °C
2: N-Bromosuccinimide; acetic acid / tetrahydrofuran / 20 °C
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethanol; toluene / 24 h / 95 - 100 °C
With
2,6-dimethylpyridine; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); sodium carbonate; acetic acid;
In
tetrahydrofuran; ethanol; toluene;
DOI:10.1016/j.bmcl.2013.05.025
- Guidance literature:
-
Multi-step reaction with 7 steps
1: potassium carbonate / N,N-dimethyl-formamide / 144 h / 130 °C
2: palladium 10% on activated carbon; hydrogen / methanol; tetrahydrofuran
3: dichloromethane / 2 h / 50 °C
4: lithium hydroxide / methanol; tetrahydrofuran / 2 h / 50 °C
5: 2,6-dimethylpyridine / ethanol / 90 °C
6: N-Bromosuccinimide; acetic acid / tetrahydrofuran / 20 °C
7: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethanol; toluene / 24 h / 95 - 100 °C
With
2,6-dimethylpyridine; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; hydrogen; sodium carbonate; potassium carbonate; acetic acid; lithium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2013.05.025
