azido[tetra(p-tolyl)porphinato]iron(III)

Base Information

• Chemical Name: azido[tetra(p-tolyl)porphinato]iron(III)
• CAS No.: 43143-56-2
• Molecular Formula: C₄₈H₃₆FeN₇
• Molecular Weight: 766.708

Synonyms:

Chemical Property of azido[tetra(p-tolyl)porphinato]iron(III)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of azido[tetra(p-tolyl)porphinato]iron(III)

There total 1 articles about azido[tetra(p-tolyl)porphinato]iron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

hydrogen azide (7782-79-8) + ((5,10,15,20-tetrap-tolylporphyrinate)Fe)2O → azido[tetra(p-tolyl)porphinato]iron(III) (43143-56-2)

Guidance literature:

In chloroform; addn. of benzene soln. of HN3 to soln. of Fe complex, stirring, 1 h; mixt. allowed to stand for 24 h; evapn. in vac., crystn. from acetone/CHCl3, drying in high vac. at 40°C; elem. anal.;

Reference yield: 52.0%

azido[tetra(p-tolyl)porphinato]iron(III) (43143-56-2) → (TpCH3PP)Fe(II)(Py)2 (62612-73-1) + ((5,10,15,20-tetrap-tolylporphyrinate)Fe)2O

Guidance literature:

With pyridine; In tetrahydrofuran; byproducts: N2; Irradiation (UV/VIS); (Ar); UV irradn. (high pressure Hg lamp) in presence of C5H5N, 1 h; evapn. in vac., residue suspended in C5H5N; filtering, drying in high vac. at 40°C; elem. anal.;

Reference yield: 52.0%

azido[tetra(p-tolyl)porphinato]iron(III) (43143-56-2) → ((5,10,15,20-tetrap-tolylporphyrinate)Fe)2O + μ-nitridobis[tetra(p-tolyl)porphinato]iron(III,IV)

Guidance literature:

In tetrahydrofuran; byproducts: N2; Irradiation (UV/VIS); (Ar); UV irradn. (high pressure Hg lamp), 1-2 h; ppt. filtered off under air, dried at 80°C, solid suspended in toluene; filtering, drying in high vac. at 40°C; elem. anal.;

upstream raw materials:

hydrogen azide

Downstream raw materials:

(TpCH₃PP)Fe(II)(Py)2

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 43143-56-2 azido[tetra(p-tolyl)porphinato]iron(III)

Send

Send

Metric Ton KG G Pound L ML

Send

Send