C₂₄H₂₃N₃O₃

Base Information

Chemical Name:C₂₄H₂₃N₃O₃
CAS No.:1144504-43-7
Molecular Formula:C₂₄H₂₃N₃O₃
Molecular Weight:401.465
Hs Code.:

C<sub>24</sub>H<sub>23</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₃N₃O₃

Chemical Property:

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Technology Process of C₂₄H₂₃N₃O₃

There total 5 articles about C₂₄H₂₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₂₇N₃O₃

: 1144504-43-7
C₂₄H₂₃N₃O₃

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; ethanol; at 60 ℃; for 16h;
DOI:10.1021/jm200400m

Reference yield:

: 186347-28-4
4-cyano-N-(1,1-dimethylethoxy)carbonyl-4-(2-methylphenyl)-piperidine

: 1144504-43-7
C₂₄H₂₃N₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / acetonitrile / 0.58 h / 0 °C

2: acetic acid / dichloromethane / 0.5 h / Microwave irradiation; Heating

3: water; sodium hydroxide / tetrahydrofuran; ethanol / 16 h / 60 °C

With hydrogenchloride; water; acetic acid; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jm200400m

Reference yield:

: 109-06-8
α-picoline

: 1144504-43-7
C₂₄H₂₃N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexanes / 0.5 h / -78 - -60 °C / Inert atmosphere

1.2: -60 - -20 °C / Inert atmosphere

1.3: 16 h / Reflux

2.1: trichlorophosphate / 1 h

3.1: acetic acid / dichloromethane / 0.5 h / Microwave irradiation; Heating

4.1: water; sodium hydroxide / tetrahydrofuran; ethanol / 16 h / 60 °C

With n-butyllithium; water; acetic acid; diisopropylamine; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; hexanes; ethanol; dichloromethane; 2.1: Vilsmeier formylation;
DOI:10.1021/jm200400m