1-(4-(5-phenyl-1,3,4-oxadiazolyl)phenyl)-2-pyridinylbenzoimidazole

Base Information

• Chemical Name: 1-(4-(5-phenyl-1,3,4-oxadiazolyl)phenyl)-2-pyridinylbenzoimidazole
• CAS No.: 1226878-10-9
• Molecular Formula: C₂₆H₁₇N₅O
• Molecular Weight: 415.454
• Mol file: 1226878-10-9.mol

Synonyms:

Chemical Property of 1-(4-(5-phenyl-1,3,4-oxadiazolyl)phenyl)-2-pyridinylbenzoimidazole

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(4-(5-phenyl-1,3,4-oxadiazolyl)phenyl)-2-pyridinylbenzoimidazole

There total 1 articles about 1-(4-(5-phenyl-1,3,4-oxadiazolyl)phenyl)-2-pyridinylbenzoimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2-(2'-pyridyl)benzimidazole (1137-68-4) + 2-(4-bromophenyl)-5-phenyl-1,3,4-oxadiazole (21510-43-0) → 1-(4-(5-phenyl-1,3,4-oxadiazolyl)phenyl)-2-pyridinylbenzoimidazole (1226878-10-9)

Guidance literature:

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; copper(l) iodide; 18-crown-6 ether; potassium carbonate; at 230 ℃; for 48h; Inert atmosphere;

DOI:10.1016/j.jorganchem.2010.04.037 DOI:10.1016/j.jphotochem.2010.02.010

Reference yield: 46.0%

bis(2,2'-bipyridine)dichlororuthenium(II) dihydrate + 1-(4-(5-phenyl-1,3,4-oxadiazolyl)phenyl)-2-pyridinylbenzoimidazole (1226878-10-9) → [Ru(2,2'-bipyridine)2(1-(4-5'-phenyl-1,3,4-oxadiazolylphenyl)-2-pyridinylbenzimidazole)]Cl2

Guidance literature:

In ethylene glycol; (Schlenk) Ru-complex and benzimidazole-compound were heated under N2 at 120°C for 6 h in ethylene glycol, cooled to room temp.; the solvent was distilled out, column chromy. on alumina (methanol/dichloromethane, v/v 0-5% as eluent);

DOI:10.1016/j.jorganchem.2010.04.037

upstream raw materials:

2-(2'-pyridyl)benzimidazole

2-(4-bromophenyl)-5-phenyl-1,3,4-oxadiazole