nickel(II) dibenzyldithiocarbamate

Base Information

Chemical Name:nickel(II) dibenzyldithiocarbamate
CAS No.:38542-61-9
Molecular Formula:C₃₀H₂₈N₂NiS₄
Molecular Weight:603.52
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of nickel(II) dibenzyldithiocarbamate

Chemical Property:

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Technology Process of nickel(II) dibenzyldithiocarbamate

There total 2 articles about nickel(II) dibenzyldithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55310-46-8
sodium dibenzyldithiocarbamate

: 13462-88-9
nickel dibromide

: 38542-61-9
nickel(II) dibenzyldithiocarbamate

Guidance literature:: In acetonitrile; byproducts: NaBr; 2 equiv. Na(dbtc) and 1 equiv. NiBr2 in MeCN was heated at 50°C for 4 h; react. mixt. was cooled, ppt. was dissolved in hot chlorobenzene and filtered, solvent was removed to dryness in vacuo; elem. anal.;
DOI:10.1021/ic051261i

Reference yield:

: Ni((C₆H₅CH₂)2NCS₂)3⁽¹⁺⁾*BF₄^(1-)*CCl₄ = [Ni((C₆H₅CH₂)2NCS₂)3]BF₄*CCl₄

: 38542-61-9
nickel(II) dibenzyldithiocarbamate

Guidance literature:: In acetonitrile; byproducts: Ni(2+), ((C6H5CH2)2NCS2)2; Irradiation (UV/VIS); irradiated (poly- (425-670 nm) and mono- (436 nm) chromatically); photometry; Kinetics;

Reference yield: 58.0%

: 295-37-4
1,4,8,11-Tetraazacyclotetradecane

: 38542-61-9
nickel(II) dibenzyldithiocarbamate

: [Ni(N,N-dibenzyldithiocarbamate)(1,4,8,11-tetraazacyclotetradecane)]ClO₄

Guidance literature:: In ethanol; chloroform; 1 equiv. of Ni-compd. in CHCl3 were reacted with 1 equiv. of N-compd. in96% EtOH, reflux for 10 h; soln. was filtered, kept for a few days, recrystn. from CHCl3 with adding of MeOH or hexane, crystals were washed with MeOH or hexane, dried under an IR lamp at 40 °C, elem. anal.;
DOI:10.1016/j.poly.2007.09.024