(CH₂CHCHCHCHOHC₆H₅)Fe(CO)3

Base Information

• Chemical Name: (CH₂CHCHCHCHOHC₆H₅)Fe(CO)3
• CAS No.: 67072-06-4
• Molecular Formula: C₁₄H₁₂FeO₄
• Molecular Weight: 300.094

Synonyms:

Chemical Property of (CH₂CHCHCHCHOHC₆H₅)Fe(CO)3

Chemical Property:

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Technology Process of (CH₂CHCHCHCHOHC₆H₅)Fe(CO)3

There total 1 articles about (CH₂CHCHCHCHOHC₆H₅)Fe(CO)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(η4-trans-2,4-pentadiene-1-al)Fe(CO)3 → (CH2CHCHCHCHOHC6H5)Fe(CO)3 (67072-06-4,276867-00-6)

Guidance literature:

With phenylmagnesium bromide; In diethyl ether; phenyl Grignard reagent in ether was added to a soln. of complex in ether at -78°C, stirred for 1 h at -78°C (N2 atm.); satd. aq. NH4Cl was added, diluted with CH2Cl2, the oraganic layerd was washed with H2O, dried over MgSO4, concd., flash column chromy. (silica gel, hexane-ethyl acetate), oil;

DOI:10.1016/S0022-328X(99)00747-0

Reference yield: 73.0%

(CH2CHCHCHCHOHC6H5)Fe(CO)3 (67072-06-4,276867-00-6) → C5H6C6H5Fe(CO)3(1+)

Guidance literature:

With tetrafluoroboric acid; In acetic anhydride; to a Schlenk flask under N2 at 5°C was added complex and Ac2O, then HBF4 was added, the mixt. was stirred at 5°C for 1 h; ether was added, ppt. was filtered, dried in vac.;

DOI:10.1016/S0022-328X(99)00747-0

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