CrPh₃(o-SCD₃C₆H₄P)(N(Me)P(o-SCD₃C₆H₄)2(o-SCD₃C₆H₄))

Base Information

Chemical Name:CrPh₃(o-SCD₃C₆H₄P)(N(Me)P(o-SCD₃C₆H₄)2(o-SCD₃C₆H₄))
CAS No.:892415-97-3
Molecular Formula:C₄₇H₄₆CrNP₂S₄
Molecular Weight:879.001
Hs Code.:

CrPh<sub>3</sub>(o-SCD<sub>3</sub>C<sub>6</sub>H<sub>4</sub>P)(N(Me)P(o-SCD<sub>3</sub>C<sub>6</sub>H<sub>4</sub>)2(o-SCD<sub>3</sub>C<sub>6</sub>H<sub>4</sub>))

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Suppliers and Price of CrPh₃(o-SCD₃C₆H₄P)(N(Me)P(o-SCD₃C₆H₄)2(o-SCD₃C₆H₄))

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Chemical Property of CrPh₃(o-SCD₃C₆H₄P)(N(Me)P(o-SCD₃C₆H₄)2(o-SCD₃C₆H₄))

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Technology Process of CrPh₃(o-SCD₃C₆H₄P)(N(Me)P(o-SCD₃C₆H₄)2(o-SCD₃C₆H₄))

There total 1 articles about CrPh₃(o-SCD₃C₆H₄P)(N(Me)P(o-SCD₃C₆H₄)2(o-SCD₃C₆H₄)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1234-62-4
triphenyltris(tetrahydrofuran)chromium(III)

: 892415-94-0
(o-CD₃SC₆H₄)2PN(CH₃)P(o-CD₃SC₆H₄)2

: 892415-97-3
CrPh₃(o-SCD₃C₆H₄P)(N(Me)P(o-SCD₃C₆H₄)2(o-SCD₃C₆H₄))

Guidance literature:: In dichloromethane; byproducts: tetrahydrofuran; (N2); using Schlenk techniques; dissolving of MeN(P(C6H4SCD3))2 in CH2Cl2; addn. of slurry of CrPh3(THF)3 in THF; stirring for 5 min; removal of volatiles in vac., addn. of CH2Cl2; removal of solvent in vac., dissolving in CH2Cl2; addn. of petroleum ether; storage at -35°C overnight; filtration, recrystn. from CH2Cl2/petroleum ether, filtration, drying under vac.; elem. anal.;
DOI:10.1021/om0506062