3-phenoxybenzyl beta-D-glucopyranosiduronic acid

Base Information

Chemical Name:3-phenoxybenzyl beta-D-glucopyranosiduronic acid
CAS No.:65658-93-7
Molecular Formula:C19H20 O8
Molecular Weight:376.3573
Hs Code.:

Synonyms:

Suppliers and Price of 3-phenoxybenzyl beta-D-glucopyranosiduronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 3-phenoxybenzyl beta-D-glucopyranosiduronic acid

Chemical Property:

Vapor Pressure:5.28E-16mmHg at 25°C
Boiling Point:615.4°C at 760 mmHg
Flash Point:221.6°C
Density:1.48g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-phenoxybenzyl beta-D-glucopyranosiduronic acid

There total 2 articles about 3-phenoxybenzyl beta-D-glucopyranosiduronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 940867-20-9
methyl 2,3,4-tri-O-acetyl-1-(3-phenoxybenzyl)-β-D-glucopyranouronate

: 65658-93-7
1-(3-phenoxybenzyl)-β-D-glucuronide

Guidance literature:: methyl 2,3,4-tri-O-acetyl-1-(3-phenoxybenzyl)-β-D-glucopyranouronate; With sodium methylate; In methanol; at 20 ℃; for 24h;

With barium dihydroxide; In methanol; at 20 ℃; for 24h; Further stages.;
DOI:10.1021/jf063282g

Reference yield:

: 3082-96-0,5432-32-6,7355-18-2,19231-41-5,30628-06-9,30628-07-0,40268-90-4,40268-95-9,40269-24-7,104195-05-3,108032-41-3
methyl 1,2,3,4-tetra-O-acetyl-α,β-D-glucopyranosyluronate

: 65658-93-7
1-(3-phenoxybenzyl)-β-D-glucuronide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 76 percent / hydrobromic acid / CH₂Cl₂; acetic acid / 3 h / 20 °C

2.1: 55 percent / silver trifluoromethanesulfonate; tetramethylurea / CH₂Cl₂ / 12 h / -20 °C

3.1: sodium methoxide / methanol / 24 h / 20 °C

3.2: 40 percent / Ba(OH)2 / methanol / 24 h / 20 °C

With hydrogen bromide; sodium methylate; silver trifluoromethanesulfonate; tetramethylurea; In methanol; dichloromethane; acetic acid; 2.1: Koenigs-Knorr reaction;
DOI:10.1021/jf063282g

Reference yield:

: [3-(2-aminoethyl)dithio]propionic acid hydrochloride

: 65658-93-7
1-(3-phenoxybenzyl)-β-D-glucuronide

: 940867-21-0
C₂₄H₂₉NO₉S₂

Guidance literature:: 1-(3-phenoxybenzyl)-β-D-glucuronide; With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 4 ℃;

[3-(2-aminoethyl)dithio]propionic acid hydrochloride; With triethylamine; In N,N-dimethyl-formamide; at 4 ℃; Further stages.;
DOI:10.1021/jf063282g