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2-(1-chlorocyclohexyl)-2-nitrosoethanol

Base Information
  • Chemical Name:2-(1-chlorocyclohexyl)-2-nitrosoethanol
  • CAS No.:101210-87-1
  • Molecular Formula:C16H28Cl2N2O4
  • Molecular Weight:383.315
  • Hs Code.:
2-(1-chlorocyclohexyl)-2-nitrosoethanol

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Chemical Property of 2-(1-chlorocyclohexyl)-2-nitrosoethanol
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Technology Process of 2-(1-chlorocyclohexyl)-2-nitrosoethanol

There total 2 articles about 2-(1-chlorocyclohexyl)-2-nitrosoethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogenchloride; 1-methylbutyl nitrite; In acetic acid; 1.) ice-salt bath, 30 min, 2.) -78 deg C, 10 min;
Guidance literature:
Multi-step reaction with 2 steps
1: 70 percent / sodium dihydrobisethoxymethoxyaluminate / diethyl ether; benzene / 0 deg C, r.t., 6 h
2: 43 percent / 2-pentyl nitrite, conc. hydrochloric acid / acetic acid / 1.) ice-salt bath, 30 min, 2.) -78 deg C, 10 min
With hydrogenchloride; 1-methylbutyl nitrite; sodium bis(2-methoxyethoxy)aluminium dihydride; In diethyl ether; acetic acid; benzene;
Guidance literature:
With ammonia; r.t., 3 days, reflux, 1.5 h, in NH3;
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