Cp₂Zr(N(t-Bu)C=N(m-Tol)N(m-Tol))

Base Information

• Chemical Name: Cp₂Zr(N(t-Bu)C=N(m-Tol)N(m-Tol))
• CAS No.: 344954-40-1
• Molecular Formula: C₂₉H₃₃N₃Zr
• Molecular Weight: 514.825

Synonyms:

Chemical Property of Cp₂Zr(N(t-Bu)C=N(m-Tol)N(m-Tol))

Chemical Property:

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Technology Process of Cp₂Zr(N(t-Bu)C=N(m-Tol)N(m-Tol))

There total 2 articles about Cp₂Zr(N(t-Bu)C=N(m-Tol)N(m-Tol)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

[(C5H5)2ZrN(C(CH3)3)C(NSi(CH3)3)N(Si(CH3)3)] + N,N'-bis(m-methylphenyl)carbodiimide (726-28-3) → Cp2Zr(N(t-Bu)C=N(m-Tol)N(m-Tol)) (344954-40-1)

Guidance literature:

In benzene-d6; byproducts: Me3SiN=C=NSiMe3; (inert gas); an NMR tube charged with complex, 1,4-dimethoxybenzene and C6D6; carbodiimide added; not isolated, detected by NMR;

DOI:10.1021/om010091o

Reference yield: 72.0%

bis(cyclopentadienyl)(tert-butylimido)(tetrahydrofuran)zirconium(IV) + N,N'-bis(m-methylphenyl)carbodiimide (726-28-3) → Cp2Zr(N(t-Bu)C=N(m-Tol)N(m-Tol)) (344954-40-1)

Guidance literature:

In benzene; byproducts: C4H8O; (inert gas); carbodiimide added dropwise to complex soln., stirred at 25°C for 20 min; evapd. (vac.), crystd. from benzene layered with hexanes at 25°C for 2 d; elem. anal.;

DOI:10.1021/om010091o

upstream raw materials:

N,N'-bis(m-methylphenyl)carbodiimide

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