1,2,4-Benzenetriol, 5-methoxy-3-(8,11,14-pentadecatrienyl)-, (Z,Z)-

Base Information

Chemical Name:1,2,4-Benzenetriol, 5-methoxy-3-(8,11,14-pentadecatrienyl)-, (Z,Z)-
CAS No.:105018-77-7
Molecular Formula:C22H32O4
Molecular Weight:360.494
Hs Code.:
Mol file:105018-77-7.mol

Synonyms:

Suppliers and Price of 1,2,4-Benzenetriol, 5-methoxy-3-(8,11,14-pentadecatrienyl)-, (Z,Z)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,4-Benzenetriol, 5-methoxy-3-(8,11,14-pentadecatrienyl)-, (Z,Z)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2,4-Benzenetriol, 5-methoxy-3-(8,11,14-pentadecatrienyl)-, (Z,Z)-

There total 20 articles about 1,2,4-Benzenetriol, 5-methoxy-3-(8,11,14-pentadecatrienyl)-, (Z,Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 123707-12-0
1,2,4-triacetoxy-5-methoxy-3(8'Z,11'Z)-pentadeca-8',11',14'-trienylbenzene

: 105018-77-7
5-methoxy-3-<(8'Z,11'Z)-pentadeca-8',11',14'-trienyl>benzene-1,2,4-triol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 0.25h;

Reference yield:

: 3990-05-4
ethyl 6-formylhexanoate

: 105018-77-7
5-methoxy-3-<(8'Z,11'Z)-pentadeca-8',11',14'-trienyl>benzene-1,2,4-triol

Guidance literature:: Multi-step reaction with 10 steps

2: 95 percent / H₂SO₄ / 16 h / Heating

3: 100 percent / LiAlH₄ / diethyl ether / 3 h / 25 °C

4: 100 percent / pyridine / toluene / 3 h / Heating

5: 90 percent / CrO₃ / acetic acid; H₂O / 1.5 h

6: 91 percent / H₂SO₄ / 12 h / 25 °C

7: 77 percent / H₂ / 10percent Pd/C / ethyl acetate / 2 h

8: 100 percent / pyridinium chlorochromate, NaOAc / CH₂Cl₂ / 3 h

9: 1) BuLi 2) HMPA / 1) THF, -78 deg C, 0.5 h, 2) THF, -78 deg C, 2 h

10: 100 percent / LiAlH₄ / tetrahydrofuran / 0.17 h / 25 °C

With pyridine; chromium(VI) oxide; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; n-butyllithium; sulfuric acid; hydrogen; sodium acetate; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetic acid; ethyl acetate; toluene;

Reference yield:

: 52483-40-6
8-(3',5'-Dimethoxyphenyl)octansaeure

: 105018-77-7
5-methoxy-3-<(8'Z,11'Z)-pentadeca-8',11',14'-trienyl>benzene-1,2,4-triol

Guidance literature:: Multi-step reaction with 9 steps

1: 95 percent / H₂SO₄ / 16 h / Heating

2: 100 percent / LiAlH₄ / diethyl ether / 3 h / 25 °C

3: 100 percent / pyridine / toluene / 3 h / Heating

4: 90 percent / CrO₃ / acetic acid; H₂O / 1.5 h

5: 91 percent / H₂SO₄ / 12 h / 25 °C

6: 77 percent / H₂ / 10percent Pd/C / ethyl acetate / 2 h

7: 100 percent / pyridinium chlorochromate, NaOAc / CH₂Cl₂ / 3 h

8: 1) BuLi 2) HMPA / 1) THF, -78 deg C, 0.5 h, 2) THF, -78 deg C, 2 h

9: 100 percent / LiAlH₄ / tetrahydrofuran / 0.17 h / 25 °C

With pyridine; chromium(VI) oxide; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; n-butyllithium; sulfuric acid; hydrogen; sodium acetate; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetic acid; ethyl acetate; toluene;