PdCl(C₆H₄(NCH₂CH₂N(C₂H₅)2)NNC₆H₄Cl)

Base Information

• Chemical Name: PdCl(C₆H₄(NCH₂CH₂N(C₂H₅)2)NNC₆H₄Cl)
• CAS No.: 1356826-20-4
• Molecular Formula: C₁₈H₂₂Cl₂N₄Pd
• Molecular Weight: 471.725
• Mol file: 1356826-20-4.mol

Synonyms:

Chemical Property of PdCl(C₆H₄(NCH₂CH₂N(C₂H₅)2)NNC₆H₄Cl)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of PdCl(C₆H₄(NCH₂CH₂N(C₂H₅)2)NNC₆H₄Cl)

There total 1 articles about PdCl(C₆H₄(NCH₂CH₂N(C₂H₅)2)NNC₆H₄Cl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

sodium tetrachloropalladate(II) + C6H4(NHCH2CH2N(C2H5)2)NNC6H4Cl (1356826-23-7) → PdCl(C6H4(NCH2CH2N(C2H5)2)NNC6H4Cl) (1356826-20-4)

Guidance literature:

In methanol; soln. of 1N-(N,N-diethylaminoethyl)-2-(4-chlorophenyl)azoaniline in MeOHadded to MeOH soln. of Na2PdCl4; stirred for 4 h; ppt. separated by filtration; purified by column chromy. using silica gel (benzene:MeCN 95:5) eluent; solvent evapd.; elem. anal.;

DOI:10.1016/j.poly.2011.11.026

upstream raw materials:

C₆H₄(NHCH₂CH₂N(C₂H₅)2)NNC₆H₄Cl

Refernces