H-(C₂-1,3-C₆H₄)6-C₂H

Base Information

Chemical Name:H-(C₂-1,3-C₆H₄)6-C₂H
CAS No.:1352435-20-1
Molecular Formula:C₅₀H₂₆
Molecular Weight:626.756
Hs Code.:

H-(C<sub>2</sub>-1,3-C<sub>6</sub>H<sub>4</sub>)6-C<sub>2</sub>H

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of H-(C₂-1,3-C₆H₄)6-C₂H

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Technology Process of H-(C₂-1,3-C₆H₄)6-C₂H

There total 9 articles about H-(C₂-1,3-C₆H₄)6-C₂H which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₀H₃₄Si₂

: 1352435-20-1
H-(C₂-1,3-C₆H₄)6-C₂H

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / Inert atmosphere

2.2: 48 h / Reflux; Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; 2.1: Sonogashira coupling / 2.2: Sonogashira coupling;
DOI:10.1021/ja208444c

Reference yield:

: C₅₆H₄₂Si₂

: 1352435-20-1
H-(C₂-1,3-C₆H₄)6-C₂H

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 0.25h;
DOI:10.1021/ja208444c

Reference yield:

: 914673-80-6
1,2-bis(3-ethynylphenyl)ethyne

: 1352435-20-1
H-(C₂-1,3-C₆H₄)6-C₂H

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / Inert atmosphere

1.2: 48 h / Reflux; Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / Inert atmosphere

3.2: 48 h / Reflux; Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; 1.1: Sonogashira coupling / 1.2: Sonogashira coupling / 3.1: Sonogashira coupling / 3.2: Sonogashira coupling;
DOI:10.1021/ja208444c