1,2-Cyclopropanedicarboxylic acid, 1,2-dicyano-, dimethyl ester, cis-

Base Information

• Chemical Name: 1,2-Cyclopropanedicarboxylic acid, 1,2-dicyano-, dimethyl ester, cis-
• CAS No.: 105020-43-7
• Molecular Formula: C₉H₈N₂O₄
• Molecular Weight: 208.174
• Mol file: 105020-43-7.mol

Synonyms:

Chemical Property of 1,2-Cyclopropanedicarboxylic acid, 1,2-dicyano-, dimethyl ester, cis-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2-Cyclopropanedicarboxylic acid, 1,2-dicyano-, dimethyl ester, cis-

There total 2 articles about 1,2-Cyclopropanedicarboxylic acid, 1,2-dicyano-, dimethyl ester, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl cis-3,4-dicyano-6,6,10,10-tetramethyl-1-thiaspiro[4.5]decane-3,4-dicarboxylate → 2,2,6,6-tetramethylcyclohexanethione (63702-84-1) + cis-1,2-Dicyan-1,2-cyclopropandicarbonsaeure-dimethylester (105020-43-7) + trans-1,2-Dicyan-1,2-cyclopropandicarbonsaeure-dimethylester (105020-42-6)

Guidance literature:

In chloroform-d1; at 100 ℃; for 3h; Title compound not separated from byproducts;

DOI:10.1016/j.tet.2005.02.062

Reference yield:

dimethyl trans-3,4-dicyano-6,6,10,10-tetramethyl-1-thiaspiro[4.5]decane-3,4-dicarboxylate → 2,2,6,6-tetramethylcyclohexanethione (63702-84-1) + cis-1,2-Dicyan-1,2-cyclopropandicarbonsaeure-dimethylester (105020-43-7) + trans-1,2-Dicyan-1,2-cyclopropandicarbonsaeure-dimethylester (105020-42-6)

Guidance literature:

In chloroform-d1; at 100 ℃; for 3h; Title compound not separated from byproducts;

DOI:10.1016/j.tet.2005.02.062

Refernces