3-(4-dimethylaminophenylazo)-5-nitrobenzoindazolium iodide

Base Information

Chemical Name:3-(4-dimethylaminophenylazo)-5-nitrobenzoindazolium iodide
CAS No.:76486-23-2
Molecular Formula:C₂₁H₂₁N₆O₂*I
Molecular Weight:516.341
Hs Code.:

3-(4-dimethylaminophenylazo)-5-nitrobenzo<g>indazolium iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-dimethylaminophenylazo)-5-nitrobenzoindazolium iodide

Chemical Property:

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Technology Process of 3-(4-dimethylaminophenylazo)-5-nitrobenzoindazolium iodide

There total 4 articles about 3-(4-dimethylaminophenylazo)-5-nitrobenzoindazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-Nitro-1H-benzo[g]indazole-3-diazonium; dihydrogen phosphate

: 76486-23-2
3-(4-dimethylaminophenylazo)-5-nitrobenzoindazolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. H₂SO₄ / 1.5 h / 0 °C

2: 1) MgO, 2) KI / 1) chlorobenzene, 110 deg C, 4 h, 2) H₂O

With magnesium oxide; potassium iodide; In sulfuric acid;

Reference yield:

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 76486-23-2
3-(4-dimethylaminophenylazo)-5-nitrobenzoindazolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. H₂SO₄ / 1.5 h / 0 °C

2: 1) MgO, 2) KI / 1) chlorobenzene, 110 deg C, 4 h, 2) H₂O

With magnesium oxide; potassium iodide; In sulfuric acid;

Reference yield:

: 67122-20-7
3-amino-5-nitrobenzoindazole

: 76486-23-2
3-(4-dimethylaminophenylazo)-5-nitrobenzoindazolium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: orthophosphoric acid, NaNO₂ / 2 h / 0 °C

2: aq. H₂SO₄ / 1.5 h / 0 °C

3: 1) MgO, 2) KI / 1) chlorobenzene, 110 deg C, 4 h, 2) H₂O

With phosphoric acid; magnesium oxide; potassium iodide; sodium nitrite; In sulfuric acid;