CH₃C₆H₄SO₂NC₄H₆(OSi(CH₃)3)CHCHCH₂Sn(C₄H₉)3

Base Information

Chemical Name:CH₃C₆H₄SO₂NC₄H₆(OSi(CH₃)3)CHCHCH₂Sn(C₄H₉)3
CAS No.:412358-01-1
Molecular Formula:C₂₉H₅₃NO₃SSiSn
Molecular Weight:642.606
Hs Code.:

CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>SO<sub>2</sub>NC<sub>4</sub>H<sub>6</sub>(OSi(CH<sub>3</sub>)3)CHCHCH<sub>2</sub>Sn(C<sub>4</sub>H<sub>9</sub>)3

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of CH₃C₆H₄SO₂NC₄H₆(OSi(CH₃)3)CHCHCH₂Sn(C₄H₉)3

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Technology Process of CH₃C₆H₄SO₂NC₄H₆(OSi(CH₃)3)CHCHCH₂Sn(C₄H₉)3

There total 2 articles about CH₃C₆H₄SO₂NC₄H₆(OSi(CH₃)3)CHCHCH₂Sn(C₄H₉)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 17955-46-3
trimethylsilyltributyltin

: 202974-97-8
4-Methyl-N-(2-oxo-ethyl)-N-((E)-penta-2,4-dienyl)-benzenesulfonamide

: 412358-01-1
CH₃C₆H₄SO₂NC₄H₆(OSi(CH₃)3)CHCHCH₂Sn(C₄H₉)3

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; In N,N-dimethyl-formamide; under Ar atm. to soln. Ni(cod)2 in DMF Me3SiSnBu3 was added and stirred at 0°C for 10 min, soln. 1,3-diene in DMF was added and stirred at room temp. for 2 h; solvent was removed, residue was purified by chromy. on silica (hexane-Et2O + 1 % Et3N);
DOI:10.1016/j.jorganchem.2006.03.047

Reference yield:

: 17955-46-3
trimethylsilyltributyltin

: 202974-97-8
4-Methyl-N-(2-oxo-ethyl)-N-((E)-penta-2,4-dienyl)-benzenesulfonamide

: CH₃C₆H₄SO₂NC₄H₆(OH)CHCHCH₂Sn(C₄H₉)3

: 412358-02-2
CH₃C₆H₄SO₂NC₄H₆(OH)CHCHCH₂Sn(C₄H₉)3

: CH₃C₆H₄SO₂NC₄H₆(OSi(CH₃)3)CHCHCH₂Sn(C₄H₉)3

: 412358-01-1
CH₃C₆H₄SO₂NC₄H₆(OSi(CH₃)3)CHCHCH₂Sn(C₄H₉)3

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; Dimethyl(phenyl)phosphine; In N,N-dimethyl-formamide; under Ar atm. to soln. Ni(cod)2 in DMF PMe2Ph was added and stirred at 0°C for 20 min, Me3SiSnBu3 was added and stirred at 0°C for10 min, soln. 1,3-diene in DMF was added and stirred at room temp. for 2 h; solvent was removed, residue was purified by chromy. on silica (hexane-Et2O + 1 % Et3N) - E- and Z-isomers were not separated;
DOI:10.1016/j.jorganchem.2006.03.047