Technology Process of C17H17NO2
There total 4 articles about C17H17NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trimethylaluminum / 5,5-dimethyl-1,3-cyclohexadiene / 16 h / Sealed tube; Inert atmosphere; Heating
2: silica gel / Inert atmosphere
With
trimethylaluminum; silica gel;
In
5,5-dimethyl-1,3-cyclohexadiene;
1: Diels-Alder reaction;
DOI:10.1021/ol203030a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: camphor-10-sulfonic acid / dichloromethane / 0.08 h / 20 °C / Inert atmosphere
2: trimethylaluminum / 5,5-dimethyl-1,3-cyclohexadiene / 16 h / Sealed tube; Inert atmosphere; Heating
3: silica gel / Inert atmosphere
With
camphor-10-sulfonic acid; trimethylaluminum; silica gel;
In
5,5-dimethyl-1,3-cyclohexadiene; dichloromethane;
2: Diels-Alder reaction;
DOI:10.1021/ol203030a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane / 0.75 h / -78 °C / Inert atmosphere
1.2: 3 h / -78 - 20 °C / Inert atmosphere
2.1: camphor-10-sulfonic acid / dichloromethane / 0.08 h / 20 °C / Inert atmosphere
3.1: trimethylaluminum / 5,5-dimethyl-1,3-cyclohexadiene / 16 h / Sealed tube; Inert atmosphere; Heating
4.1: silica gel / Inert atmosphere
With
n-butyllithium; camphor-10-sulfonic acid; trimethylaluminum; silica gel;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; 5,5-dimethyl-1,3-cyclohexadiene; hexane; dichloromethane;
3.1: Diels-Alder reaction;
DOI:10.1021/ol203030a
