Technology Process of C20H18F4O5S
There total 11 articles about C20H18F4O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Resolution of racemate;
- Guidance literature:
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Multi-step reaction with 10 steps
1: potassium carbonate / tetrahydrofuran
2: lithium aluminium tetrahydride / tetrahydrofuran
3: potassium tert-butylate / tetrahydrofuran
4: Dess-Martin periodane / dichloromethane
5: trimethylsilyl trifluoromethanesulfonate
6: 3-chloro-benzenecarboperoxoic acid / dichloromethane
7: boron trifluoride diethyl etherate / dichloromethane
8: triethylamine / dichloromethane
9: potassium tert-butylate / tetrahydrofuran
10: ozone / dichloromethane
With
lithium aluminium tetrahydride; trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; potassium tert-butylate; potassium carbonate; Dess-Martin periodane; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
1: |Michael Addition;
DOI:10.1016/j.bmcl.2012.11.047
- Guidance literature:
-
Multi-step reaction with 8 steps
1: potassium tert-butylate / tetrahydrofuran
2: Dess-Martin periodane / dichloromethane
3: trimethylsilyl trifluoromethanesulfonate
4: 3-chloro-benzenecarboperoxoic acid / dichloromethane
5: boron trifluoride diethyl etherate / dichloromethane
6: triethylamine / dichloromethane
7: potassium tert-butylate / tetrahydrofuran
8: ozone / dichloromethane
With
trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; potassium tert-butylate; Dess-Martin periodane; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.11.047