C₂₃H₂₅ClN₂O₃S₂

Base Information

Chemical Name:C₂₃H₂₅ClN₂O₃S₂
CAS No.:1374354-72-9
Molecular Formula:C₂₃H₂₅ClN₂O₃S₂
Molecular Weight:477.048
Hs Code.:

C<sub>23</sub>H<sub>25</sub>ClN<sub>2</sub>O<sub>3</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₂₃H₂₅ClN₂O₃S₂

Chemical Property:

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Technology Process of C₂₃H₂₅ClN₂O₃S₂

There total 12 articles about C₂₃H₂₅ClN₂O₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₃₆ClNO₄SSi

: 1374354-72-9
C₂₃H₂₅ClN₂O₃S₂

Guidance literature:: Multi-step reaction with 5 steps

1: Lawessons reagent; pyridine / toluene / 100 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran

3: thionyl chloride / toluene

4: N-ethyl-N,N-diisopropylamine / acetonitrile

5: water; sodium hydroxide / ethanol

With Lawessons reagent; pyridine; thionyl chloride; tetrabutyl ammonium fluoride; water; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; ethanol; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067

Reference yield:

: C₁₁H₁₂BrClO₂

: 1374354-72-9
C₂₃H₂₅ClN₂O₃S₂

Guidance literature:: Multi-step reaction with 7 steps

1: sodium diformamide

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform

3: Lawessons reagent; pyridine / toluene / 100 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran

5: thionyl chloride / toluene

6: N-ethyl-N,N-diisopropylamine / acetonitrile

7: water; sodium hydroxide / ethanol

With Lawessons reagent; pyridine; thionyl chloride; sodium diformamide; tetrabutyl ammonium fluoride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; ethanol; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067

Reference yield:

: 18791-75-8
4-Bromothiophen-2-aldehyde

: 1374354-72-9
C₂₃H₂₅ClN₂O₃S₂

Guidance literature:: Multi-step reaction with 10 steps

1: sodium tetrahydroborate / methanol

2: 1H-imidazole

3: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II)

4: n-butyllithium / tetrahydrofuran

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform

6: Lawessons reagent; pyridine / toluene / 100 °C

7: tetrabutyl ammonium fluoride / tetrahydrofuran

8: thionyl chloride / toluene

9: N-ethyl-N,N-diisopropylamine / acetonitrile

10: water; sodium hydroxide / ethanol

With Lawessons reagent; pyridine; 1H-imidazole; sodium tetrahydroborate; n-butyllithium; thionyl chloride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); tetrabutyl ammonium fluoride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067