(2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)Fe(N₂)2

Base Information

Chemical Name:(2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)Fe(N₂)2
CAS No.:1365064-41-0
Molecular Formula:C₃₅H₄₈FeN₈
Molecular Weight:636.667
Hs Code.:

(2,6-(2,6-(i)Pr<sub>2</sub>-C<sub>6</sub>H<sub>3</sub>N=CMe)2-4-Me<sub>2</sub>N-C<sub>5</sub>H<sub>2</sub>N)Fe(N<sub>2</sub>)2

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Chemical Property of (2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)Fe(N₂)2

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Technology Process of (2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)Fe(N₂)2

There total 1 articles about (2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)Fe(N₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 1365064-34-1
(2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)FeCl₂

: 7727-37-9
nitrogen

: 1365064-41-0
(2,6-(2,6-(i)Pr₂-C₆H₃N=CMe)2-4-Me₂N-C₅H₂N)Fe(N₂)2

Guidance literature:: With Na; Hg; In tetrahydrofuran; toluene; under N2; by a react. of Fe-contg. compd. (0.77 mmol) in toluene and THFwith N2 (1 atm) in the presence of sodium amalgam (prepd. from Hg and N a in toluene); stirring for 3 h; the mixt. was decanted away from the amalgam and concd. in vac. to remove THF; the residue was extd. with pentane, filtered through a pad of Celite and concd.; the soln. was stored at -35°C and deposited as solid;
DOI:10.1021/om201212m